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Powder micro-XRD of small particles

Published online by Cambridge University Press:  29 February 2012

Joseph R. Swider
Joseph R. Swider*
Affiliation:
McCrone Associates, Inc., Westmont, Illinois 60559
*
a)Electronic mail: [email protected]
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Abstract

The increasing use of microanalysis techniques to analyze particles has demanded more rapid phase identification methods for samples in the 10 μm size range. The XRD analysis of such particles is routinely accomplished using a Rigaku combination instrument combined with particle handling methods. Several case studies show the variety of material analysis problems that can be solved with this technique including identification of multiple mineral phases, corrosion components, and paint samples.

Keywords

micro-XRDparticle phase analysismicroanalysis
Type
Laboratory Note
Information
Powder Diffraction , Volume 25 , Issue 1 , March 2010 , pp. 68 - 71
Copyright
Copyright © Cambridge University Press 2010

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References

Castelnau, O., Ungar, T., Drakopoulos, M., Snigirev, A., Snigireva, I., Schorer, C., Chauveau, T., and Bacroix, B. (2000). “Single grain analysis of strain hardening and internal stresses in cold rolled IF-Ti steel with a new high-resolution microdiffraction technique,” Key Eng. Mater. KEMAEY 177–180, 147–152 .10.4028/www.scientific.net/KEM.177-180.147CrossRefGoogle Scholar
Fujiwara, A., Ishii, K., Watanuki, T., Suematsu, H., Nakao, H., Ohwada, K., Fujii, Y., Murakami, Y., Mori, T., Kawada, H., Kikegawa, T., Shimomura, O., Matsubara, T., Hanabusa, H., Daicho, S., Kitamura, S., and Katayama, C. (2000). “Synchrotron radiation X-ray powder diffractometer with a cylindrical imaging plate,” J. Appl. Crystallogr. JACGAR 33, 1241–1245 .10.1107/S0021889800009286CrossRefGoogle Scholar
Nel, P., Lau, D., and Hay, D. (2006). “Non-destructive micro-X-ray diffraction analysis of painted artefacts: Determination of detection limits for the chromium oxide-zinc oxide matrix,” Nucl. Instrum. Methods Phys. Res. B NIMBEU 251, 489–495 .10.1016/j.nimb.2006.07.003CrossRefGoogle Scholar
Salbu, B., Janssens, K., Lind, O. C., Simionovici, A., Krekling, T., Drakopoulos, M., Snigireva, I., and Snigirev, A. (2002). “SR-based X-ray microbeam techniques utilized for solid-state speciation of U in fuel particles,” Proceedings of Actinide XAS Workshop (unpublished), p. 119.Google Scholar
Salbu, B., Krekling, T., Lind, O. C., Oughton, D. H., Drakopoulos, M., Simionovici, A., Snigireva, I., Snigirev, A., Weitkamp, T., Adams, F., Janssens, K., and Kashparov, V. A. (2001). “High energy X-ray microscopy for characterisation of fuel particles,” Nucl. Instrum. Methods Phys. Res. A NIMAER 467–468, 1249–1252 .10.1016/S0168-9002(01)00641-6CrossRefGoogle Scholar
Swider, J. R. (2009). “Micro powder X-ray diffraction in the laboratory,” Modern Microscopy, 〈http://www.modernmicroscopy.com/main.asp?article=94〉.Google Scholar