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Microstructure, texture, and enhanced mechanical properties of an extruded Mg–rare earth alloy after hot compression

Published online by Cambridge University Press:  10 December 2015

Yi Ping Wu*
Affiliation:
School of Materials Science and Engineering, Central South University, Changsha City, 410083, Hunan Province, People's Republic of China; and Institute for Frontier Materials, Geelong Technology Precinct, Deakin University, Geelong, Victoria 3220, Australia
Xin Ming Zhang
Affiliation:
School of Materials Science and Engineering, Central South University, Changsha City 410083, Hunan Province, People's Republic of China; and The Key Laboratory of Nonferrous Metal Materials Science and Engineering, Central South University, Changsha City, 410083, Hunan Province, People's Republic of China
Yun Lai Deng
Affiliation:
School of Materials Science and Engineering, Central South University, Changsha City 410083, Hunan Province, People's Republic of China; and The Key Laboratory of Nonferrous Metal Materials Science and Engineering, Central South University, Changsha City, 410083, Hunan Province, People's Republic of China
Chang Ping Tang
Affiliation:
School of Materials Science and Engineering, Central South University, Changsha City 410083, Hunan Province, People's Republic of China; and The Key Laboratory of Nonferrous Metal Materials Science and Engineering, Central South University, Changsha City, 410083, Hunan Province, People's Republic of China
*
a) Address all correspondence to this author. e-mail: [email protected]
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Abstract

An extruded Mg–8Gd–4Y–1Nd–0.5Zr alloy was preheated at 500 °C for 0.5 h and then subjected to hot compression to a true strain of 0.69 at temperature 450 °C and a strain rate of 0.2 s−1. It is observed that boundaries of small grains (∼3 μm) in the extruded alloy are decorated with irregular-shaped particles; small grains show a weak texture of three main components of $\left\langle {0001} \right\rangle //{\rm{TD}}$ , $\left\langle {11\overline 2 1} \right\rangle //{\rm{ND}}$ , and $\left\langle {10\overline 1 0} \right\rangle //{\rm{ED}}$ . Dynamic recrystallization is concurrent with dynamic precipitation of particles during hot compression, resulting in both a uniform grain structure and a redistribution of particles. The retained particles before compression keep the texture unchanged during compression, leading to the same texture type of $\left\langle {0001} \right\rangle //{\rm{TD}}$ of the compressed alloy as that of the preheated alloy. The compressed alloy exhibits a better aging hardening ability than the extruded alloy. After peak aging, the compressed alloy presents an ultimate tensile strength of 416 MPa, a yield tensile strength of 317 MPa, and an elongation of 2.7%.

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Articles
Copyright
Copyright © Materials Research Society 2015 

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Footnotes

Contributing Editor: Jürgen Eckert

References

REFERENCES

Liang, S., Guan, D., Tan, X., Chen, L., and Tang, Y.: Effect of isothermal aging on the microstructure and properties of as-cast Mg–Gd–Y–Zr alloy. Mater. Sci. Eng., A 528, 1589 (2011).Google Scholar
Tang, C.P., Yang, L., Feng, D., Deng, Y.L., and Zhang, X.M.: Investigation on microstructure and mechanical properties of a Mg–Gd–Y–Zr Alloy plate. Mater. Manuf. Processes 27, 609 (2012).CrossRefGoogle Scholar
Zhang, X.M., Tang, C.P., Deng, Y.L., Yang, L., and Liu, W.J.: Phase transformation in Mg–8Gd–4Y–Nd–Zr alloy. J. Alloys Compd. 509, 6170 (2011).Google Scholar
Bohlen, J., Yi, S., Letzig, D., and Kainer, K.U.: Effect of rare earth elements on the microstructure and texture development in magnesium–manganese alloys during extrusion. Mater. Sci. Eng., A 527, 7092 (2010).CrossRefGoogle Scholar
Mirza, F.A., Chen, D.L., Li, D.J., and Zeng, X.Q.: Effect of rare earth elements on deformation behavior of an extruded Mg–10Gd–3Y–0.5Zr alloy during compression. Mater. Des. 46, 411 (2013).CrossRefGoogle Scholar
Stanford, N. and Barnett, M.: The origin of “rare earth” texture development in extruded Mg-based alloys and its effect on tensile ductility. Mater. Sci. Eng., A 496, 399 (2008).CrossRefGoogle Scholar
Wu, W.X., Jin, L., Wang, F.H., Sun, J., Zhang, Z.Y., Ding, W.J., and Dong, J.: Microstructure and texture evolution during hot rolling and subsequent annealing of Mg–1Gd alloy. Mater. Sci. Eng., A 582, 194 (2013).Google Scholar
Zhu, T.L., Sun, J.F., Cui, C.L., Wu, R.Z., Betsofen, S., Leng, Z., Zhang, J.H., and Zhang, M.L.: Influence of Y and Nd on microstructure, texture and anisotropy of Mg–5Li–1A1 alloy. Mater. Sci. Eng., A 600, 1 (2014).CrossRefGoogle Scholar
Bohlen, J., Nürnberg, M.R., Senn, J.W., Letzig, D., and Agnew, S.R.: The texture and anisotropy of magnesium–zinc–rare earth alloy sheets. Acta Mater. 55, 2101 (2007).Google Scholar
Ball, E.A. and Prangnell, P.B.: Tensile-compressive yield asymmetries in high strength wrought magnesium alloys. Scr. Metall. Mater. 31, 111 (1994).CrossRefGoogle Scholar
Al-Samman, T. and Li, X.: Sheet texture modification in magnesium-based alloys by selective rare earth alloying. Mater. Sci. Eng., A 528, 3809 (2011).Google Scholar
Hou, X., Peng, Q., Cao, Z., Xu, S., Kamado, S., Wang, L., Wu, Y., and Wang, L.: Structure and mechanical properties of extruded Mg–Gd based alloy sheet. Mater. Sci. Eng., A 520, 162 (2009).CrossRefGoogle Scholar
Liu, X., Le, Q., Zhang, Z., Bao, L., and Cui, J.: Effects of Nd/Gd ratio on the microstructures and mechanical properties of Mg–Gd–Y–Nd–Zr alloys. Indian J. Eng. Mater. Sci. 22, 14 (2015).CrossRefGoogle Scholar
Peng, Q., Wang, J., Wu, Y., and Wang, L.: Microstructures and tensile properties of Mg–8Gd–0.6Zr–xNd–yY (x + y = 3, mass%) alloys. Mater. Sci. Eng., A 433, 133 (2006).CrossRefGoogle Scholar
Li, L., Zhang, X.M., Deng, Y.L., and Tang, C.P.: Superplasticity and microstructure in Mg–Gd–Y–Zr rolled sheet. J. Alloys Compd. 485, 295 (2009).Google Scholar
Wu, Y.P., Zhang, X.M., Deng, Y.L., Tang, C.P., and Zhong, Y.Y.: Effect of secondary extrusion on the microstructure and mechanical properties of a Mg–RE alloy. Mater. Sci. Eng., A 616, 148 (2014).Google Scholar
Farzadfar, S.A., Sanjari, M., Jung, I.H., Essadiqi, E., and Yue, S.: Role of yttrium in the microstructure and texture evolution of Mg. Mater. Sci. Eng., A 528, 6742 (2011).CrossRefGoogle Scholar
Al-Samman, T., Li, X., and Chowdhury, S.G.: Orientation dependent slip and twinning during compression and tension of strongly textured magnesium AZ31 alloy. Mater. Sci. Eng., A 527, 3450 (2010).Google Scholar
Chang, L.L., Wang, Y.N., Zhao, X., and Qi, M.: Grain size and texture effect on compression behavior of hot-extruded Mg–3Al–1Zn alloys at room temperature. Mater. Charact. 60, 991 (2009).CrossRefGoogle Scholar
Choi, S.H., Kim, J.K., Kim, B.J., and Park, Y.B.: The effect of grain size distribution on the shape of flow stress curves of Mg–3Al–1Zn under uniaxial compression. Mater. Sci. Eng., A 488, 458 (2008).Google Scholar
Dobroň, P., Chmelík, F., Yi, S., Parfenenko, K., Letzig, D., and Bohlen, J.: Grain size effects on deformation twinning in an extruded magnesium alloy tested in compression. Scr. Mater. 65, 424 (2011).Google Scholar
Wang, B., Xin, R., Huang, G., and Liu, Q.: Effect of crystal orientation on the mechanical properties and strain hardening behavior of magnesium alloy AZ31 during uniaxial compression. Mater. Sci. Eng., A 534, 588 (2012).Google Scholar
Shi, B.Q., Chen, R.S., and Ke, W.: Effects of forging processing on the texture and tensile properties of ECAEed AZ80 magnesium alloy. Mater. Sci. Eng., A 546, 323 (2012).CrossRefGoogle Scholar
Wang, S., Kang, S., and Cho, J.: Effect of hot compression and annealing on microstructure evolution of ZK60 magnesium alloys. J. Mater. Sci. 44, 5475 (2009).CrossRefGoogle Scholar
Hadorn, J.P., Hantzsche, K., Yi, S.B., Bohlen, J., Letzig, D., Wollmershauser, J., and Agnew, S.R.: Role of solute in the texture modification during hot deformation of Mg-rare earth alloys. Metall. Mater. Trans. A 43, 1347 (2012).Google Scholar
Li, L.: Deformation band and texture of a cast Mg–RE alloy under uniaxial hot compression. Mater. Sci. Eng., A 528, 7178 (2011).Google Scholar
Xia, X., Zhang, K., Li, X., Ma, M., and Li, Y.: Microstructure and texture of coarse-grained Mg–Gd–Y–Nd–Zr alloy after hot compression. Mater. Des. 44, 521 (2013).Google Scholar
Cottam, R., Robson, J., Lorimer, G., and Davis, B.: Dynamic recrystallization of Mg and Mg–Y alloys: Crystallographic texture development. Mater. Sci. Eng., A 485, 375 (2008).CrossRefGoogle Scholar
Stanford, N., Atwell, D., and Barnett, M.R.: The effect of Gd on the recrystallisation, texture and deformation behaviour of magnesium-based alloys. Acta Mater. 58, 6773 (2010).CrossRefGoogle Scholar