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Preparation of layered double hydroxide films using an electrodeposition and subsequent crystal growth method

Published online by Cambridge University Press:  23 February 2022

Noriyuki Sonoyama Open the ORCID record for Noriyuki Sonoyama [Opens in a new window] ,
Shizuka Yamada ,
Tomoki Ota ,
Haruna Inagaki ,
Patrick K. Dedetemo  and
Satoshi Yoshida
Noriyuki Sonoyama*
Affiliation:
Department of Life and Applied Chemistry, Nagoya Institute of Technology, Gokiso-cyo, Showa-ku, Nagoya 466-8555, Japan
Shizuka Yamada
Affiliation:
Department of Life and Applied Chemistry, Nagoya Institute of Technology, Gokiso-cyo, Showa-ku, Nagoya 466-8555, Japan
Tomoki Ota
Affiliation:
Department of Life and Applied Chemistry, Nagoya Institute of Technology, Gokiso-cyo, Showa-ku, Nagoya 466-8555, Japan
Haruna Inagaki
Affiliation:
Department of Life and Applied Chemistry, Nagoya Institute of Technology, Gokiso-cyo, Showa-ku, Nagoya 466-8555, Japan
Patrick K. Dedetemo
Affiliation:
Department of Life and Applied Chemistry, Nagoya Institute of Technology, Gokiso-cyo, Showa-ku, Nagoya 466-8555, Japan
Satoshi Yoshida
Affiliation:
Department of Life and Applied Chemistry, Nagoya Institute of Technology, Gokiso-cyo, Showa-ku, Nagoya 466-8555, Japan
*
*E-mail: [email protected]
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Abstract

The surface coating of a gas reaction electrode with layered double hydroxides (LDHs) featuring various electrode catalyst activities was prepared via electrodeposition and the subsequent crystal growth of LDHs. LDH formation was confirmed by X-ray diffraction and Raman scattering measurements after subsequent crystal growth on respective electrodeposited precursor films in Ni-Fe and Zn-Al LDH systems. However, the crystal growth of LDHs in Ni-Mn and Cu-Mn systems was observed on the Mg-Al LDH-electrodeposited films. LDH films were also deposited on the surface of a carbon paper electrode with a rugged surface via electrodeposition and subsequent crystal growth. Using the prepared LDH-coated carbon paper electrodes, the electrode catalytic activity for the oxygen reduction reaction (ORR) was examined. For Ni-Mn, Ni-Al and Ni-Fe LDH-coated carbon paper electrodes, the threshold voltages of the ORR decreased. Hence, the LDHs electrodeposited on a gas reaction electrode have high electrochemical catalytic activity for the ORR.

Keywords

coating on a porous electrodeelectrode catalyst for oxygen reductionelectrodepositionlayered double hydroxide (LDH)subsequent crystal growth
Type
Article
Information
Clay Minerals , Volume 56 , Issue 4 , December 2021 , pp. 284 - 291
Copyright
Copyright © The Author(s), 2022. Published by Cambridge University Press on behalf of The Mineralogical Society of Great Britain and Ireland

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Footnotes

Associate Editor: Huaming Yang

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