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A Comparison of Cellulose Extraction and ABA Pretreatment Methods for AMS 14C Dating of Ancient Wood

Published online by Cambridge University Press:  18 July 2016

J R Southon*
Affiliation:
Earth System Science Department, University of California, Irvine, California 92697, USA
A L Magana
Affiliation:
Earth System Science Department, University of California, Irvine, California 92697, USA
*
Corresponding author. Email: [email protected].
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Abstract

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We have compared accelerator mass spectrometry (AMS) radiocarbon results on wood samples at or near the limit of 14C dating, pretreated with a standard acid-base-acid (ABA) protocol, with those obtained from cellulose prepared from the same samples by several modifications of the Jayme-Wise cellulose extraction method (Green 1963). These tests were carried out to determine the most efficient way to ensure low backgrounds in 14C measurements of well-preserved ancient wood samples.

Type
Sample Preparation
Copyright
Copyright © 2010 by the Arizona Board of Regents on behalf of the University of Arizona 

References

Bird, MI, Ayliffe, LK, Fifield, LK, Turney, CSM, Cresswell, RG, Barrows, TT, David, B. 1999. Radiocarbon dating of “old” charcoal using a wet oxidation, stepped-combustion procedure. Radiocarbon 41(2):127–40.Google Scholar
Brown, TA, Nelson, DE, Matthewes, RW, Vogel, JS, Southon, JR. 1989. Radiocarbon dating of pollen by accelerator mass spectrometry. Quaternary Research 32(2):205–12.CrossRefGoogle Scholar
Cain, WF, Suess, HE. 1976. Carbon 14 in tree rings. Journal of Geophysical Research 81(21):3688–94.Google Scholar
Gaudinski, JB, Dawson, TE, Quideau, S, Schuur, EAG, Roden, JS, Trumbore, SE, Sandquist, DR, Oh, S-W, Wasylishen, RE. 2005. Comparative analysis of cellulose preparation techniques for use with 13C, 14C and 18O isotopic measurements. Analytical Chemistry 77(22):7212–24.Google Scholar
Gillespie, R. 1990. On the use of oxidation for AMS sample pretreatment. Nuclear Instruments and Methods in Physics Research B 52(3–4):345–7.Google Scholar
Gordon, G. 1982. Improved methods of analysis for chlorate, chlorite, and hypochlorite ions at the sub-mg/L level. In: Proceedings of the Water Quality Technology Conference. American Water Works Association, Nashville, Tennessee, USA. p 175–89.Google Scholar
Green, JW. 1963. Methods of Carbohydrate Chemistry. New York: Academic Press. p 921.Google Scholar
Hatté, C, Morvan, J, Noury, C, Paterne, M. 2001. Is classical acid-alkali-acid treatment responsible for contamination? An alternative proposition. Radiocarbon 43(2A):177–82.Google Scholar
Hogg, AG, Fifield, LK, Turney, CSM, Palmer, JG, Galbraith, R, Baillie, MGK. 2006. Dating ancient wood by high sensitivity liquid scintillation counting and accelerator mass spectrometry—pushing the boundaries. Quaternary Geochronology 1(4):241–8.Google Scholar
Kaczur, JJ, Cawlfield, DW. 2000. Chlorine oxygen acids and salts, chlorous acid, chlorites and chlorine dioxide. In: Kirk-Othmer Encyclopedia of Chemical Technology. 5th edition. New York: John Wiley and Sons.Google Scholar
Leavitt, SW, Danzer, SR. 1993. Method for processing small wood samples to holocellulose for stable-carbon isotope analysis. Analytical Chemistry 65(1):87–9.CrossRefGoogle Scholar
Linick, TW, Long, A, Damon, PE, Ferguson, CW. 1986. High-precision radiocarbon dating of bristlecone pine from 6554 to 5350 BC. Radiocarbon 28(2B):943–53.Google Scholar
Long, A, Kalin, RM. 1992. High-sensitivity radiocarbon dating in the 50,000 to 70,000 BP range without isotopic enrichment. Radiocarbon 34(2):351–9.CrossRefGoogle Scholar
Marra, MJ, Alloway, BV, Newnham, RM. 2006. Paleoenvironmental reconstruction of a well-preserved Stage 7 forest sequence catastrophically buried by basaltic eruptive deposits, northern New Zealand. Quaternary Science Reviews 25(17–18):2143–61.CrossRefGoogle Scholar
Pearson, GW, Stuiver, M. 1986. High-precision calibration of the radiocarbon time scale 500–2500 BC. Radiocarbon 28(2B):839–62.Google Scholar
Pigati, JS, Quade, J, Wilson, J, Jull, AJT, Lifton, NA. 2007. Development of low-background vacuum extraction and graphitization systems for 14C dating of old (40–60 ka) samples. Quaternary International 166(1):414.Google Scholar
Santos, GM, Bird, MI, Pillans, B, Fifield, LK, Alloway, BV, Chappell, J, Hausladen, PA, Arneth, A. 2001. Radiocarbon dating of wood using different pretreatment procedures: application to the chronology of Rotoehu Ash, New Zealand. Radiocarbon 43(2A):239–48.Google Scholar
Skelly, JK. 1960. The theory and practice of sodium chlorite bleaching. The Journal of the Society of Dyers and Colorists 76(8):469–79.Google Scholar
Stuiver, M, Quay, PD. 1981 Atmospheric 14C changes resulting from fossil fuel CO2 release and cosmic ray flux variability. Earth and Planetary Science 53(3):349–62.Google Scholar
Svensson, DR, Jameel, H, Chang, H-M, Kadla, JF. 2006. Inorganic reactions in chlorine dioxide bleaching of softwood kraft pulp. Journal of Wood Chemistry and Technology 26(3):201–13.Google Scholar
Turney, CSM, Fifield, LK, Palmer, JG, Hogg, AG, Baillie, MGL, Galbraith, R, Ogden, J, Lorrey, A, Tims, SG. 2007. Towards a radiocarbon calibration for oxygen isotope stage 3 using New Zealand kauri (Agathis Australis). Radiocarbon 49(2):447–57.CrossRefGoogle Scholar