No CrossRef data available.
Article contents
X-ray powder diffraction data for trelagliptin succinate, C18H20FN5O2•C4H6O4
Published online by Cambridge University Press: 23 May 2016
Abstract
Experimental X-ray powder diffraction data, unit-cell parameters, and space group for trelagliptin succinate, C18H20FN5O2•C4H6O4, are reported [a = 18.481(6), b = 8.120(4), c = 7.903(4) Å, α = 89.972(0)°, β = 97.722(4)°, γ = 90.120(0)°, unit-cell volume V = 1175.37 Å3, Z = 2, and space-group P1]. All measured lines were indexed and are consistent with the P1 space group. No detectable impurity was observed.
- Type
- New Diffraction Data
- Information
- Copyright
- Copyright © International Centre for Diffraction Data 2016
References
Harris, K. D. M. (2012). “Powder diffraction crystallography of molecular solids,” Top. Curr. Chem. 315, 133–178.CrossRefGoogle ScholarPubMed
Inagaki, N., Onouchi, H., Sano, H., Kuroda, S., and Kaku, K. (2014). “Efficacy and safety of trelagliptin, a novel once-weekly oral DPP-4 inhibitor: a phase 3, double-blind, non-inferiority study in Japanese type 2 diabetes mellitus patients,” Diabetologia
57, S328.Google Scholar
Inagaki, N., Onouchi, H., Maezawa, H., Kuroda, S., and Kaku, K. (2015). “Once-weekly trelagliptin versus daily alogliptin in Japanese patients with type 2 diabetes: a randomised, double-blind, phase 3, non-inferiority study,” Lancet Diab. Endocrinol. 3, 191–197.Google Scholar
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin: powder X-ray diffraction versus single-crystal X-ray diffraction,” Chin. Sci. Bull. 57, 3867–3871.CrossRefGoogle Scholar
Pawley, G. S. (1981). “Unit-cell refinement from powder diffraction scans,” J. Appl. Crystallogr. 14, 357–361.Google Scholar