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X-ray powder diffraction data for RuCI2(TRIPHOS)(DMSO) dichloro [bis(2-diphenylphosphinoethyl) phenylphosphine] [dimethylsulfoxide] ruthenium (II)

Published online by Cambridge University Press:  10 January 2013

Gerzon Delgado ,
A. Valentina Rivera ,
Trino Suárez  and
Bernardo Fontal
Gerzon Delgado
Affiliation:
Departamento de Química, Facultad de Ciencias, Universidad de Los Andes Mérida, Mérida 5101, Venezuela
A. Valentina Rivera
Affiliation:
Departamento de Química, Facultad de Ciencias, Universidad de Los Andes Mérida, Mérida 5101, Venezuela
Trino Suárez
Affiliation:
Departamento de Química, Facultad de Ciencias, Universidad de Los Andes Mérida, Mérida 5101, Venezuela
Bernardo Fontal
Affiliation:
Departamento de Química, Facultad de Ciencias, Universidad de Los Andes Mérida, Mérida 5101, Venezuela
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Abstract

X-ray powder diffraction data for Dichloro [bis(2-diphenylphosphinoethyl) phenylphosphine] [dimethylsulfoxide] Ruthenium (II) is reported. The powder pattern was obtained using CuKα radiation. The lattice parameters determinated by least-squares refinement for the monoclinic space group P21/c are: a = 21.073(3) Å, b = 11.970(2) Å, c = 16.889(3) Å, and β = 107.72(1)°, with M20 = 10.67 and F30 = 15.4 (0.0145, 134), and are in good agreement with those obtained from the single crystal structure determination. Observed and calculated X-ray powder diffraction data are given for the titled compound.

Type
Research Article
Information
Powder Diffraction , Volume 10 , Issue 3 , September 1995 , pp. 178 - 179
Copyright
Copyright © Cambridge University Press 1995

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References

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