Hostname: page-component-586b7cd67f-r5fsc Total loading time: 0 Render date: 2024-12-04T19:51:30.817Z Has data issue: false hasContentIssue false
  • English
  • Français

X-ray powder diffraction data for peiminine

Published online by Cambridge University Press:  29 July 2013

Dan Xiao ,
Li Li Zhang ,
Xiao Qing Wu ,
Jin Yan ,
Wei Luo  and
Hui Li
Dan Xiao
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Li Li Zhang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Xiao Qing Wu
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Jin Yan
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Wei Luo
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a) Author to whom correspondence should be addressed. Electronic mail: [email protected]
Get access Rights & Permissions [Opens in a new window]

Abstract

X-ray powder diffraction data, unit-cell parameters and space group for peiminine, C27H43NO3, are reported (a = 30.2026 Å, b = 5.8468 Å, c = 14.4344 Å, β = 96.9456°, unit-cell volume V = 2530.23 Å3, Z = 2 and space group P21). All measured lines were indexed and are consistent with the P21 space group. No detectable impurity was observed.

Keywords

X-ray powder diffractionpeiminine
Type
New Diffraction Data
Information
Powder Diffraction , Volume 28 , Issue 4 , December 2013 , pp. 312 - 314
Copyright
Copyright © International Centre for Diffraction Data 2013 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Ding, K., Lin, G., Ho, Y. P., Cheng, T. Y., and Li, P. (1996). “Prederivatization and high-performance liquid chromatographic analysisof alkaloid of bulbs of Fritillaria,” J. Pharm. Sci. 85, 1174–1179.CrossRefGoogle Scholar
Engel, G. E., Wilke, S., König, O., Harris, K. D. M., and Leusen, F. J. J. (1999). “Powder Solve a complete package for crystal structure solution from powder diffraction patterns,” J. Appl. Crystal. 32, 1169–1179.Google Scholar
Oh, H., Kang, D. G., Lee, S., Lee, Y., and Lee, H. S. (2003). “Angiotensin converting enzyme (ACE) inhibitory alkaloids from Fritillaria ussuriesis,” Planta Med. 69(6), 564–565.Google Scholar
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin: Powder X-ray diffraction versus single-crystal X-ray diffraction,” Chin. Sci. Bull. (China) 57, 3867–3871.Google Scholar
Wang, D. D., Zhu, J. Y., Wang, S., Wang, X. X., Ou, Y., Wei, D. D., and Li, X. P. (2011). “Antitussive, expectorant and anti-inflammatory alkaloids from Bulbus Fritillariae Cirrhosae,” Fitoterapia. 82, 1290–1294.Google Scholar
Xiao, C. P., Zhao, H. R., Li, P., and Xu, G. J. (1992). “Antimicrobial activity (in vitro) of the constituents of Bulbus Fritillariae ,” J. China Pharm. Univ. 23, 188–189.Google Scholar
Xu, D. M., Xu, M. L., Wang, S. Q., Hung, E. X., and Wen, X. G. (1990). “Two new steroidal alkaloids from Fritillaria ussuriensis,” J. Nat. Prod. 53, 549–552.CrossRefGoogle ScholarPubMed
Young, R. A. (1993). The Rietveld Method, IUCr Monographies of Crystallography (Wiley, Oxford).Google Scholar