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X-ray powder diffraction data for DCT (C12H12Cl2N6O4S2 • C6H15N)

Published online by Cambridge University Press:  09 June 2015

XiaoLi Ma ,
ShanShan Li ,
LiuQi Guo ,
Qing Wang  and
Hui Li
XiaoLi Ma
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
ShanShan Li
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
LiuQi Guo
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Qing Wang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]
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Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for DCT (C12H12Cl2N6O4S2 • C6H15N) are reported [a = 18.991(9) Å, b = 19.057(2) Å, c = 7.346(8) Å, α = β = γ = 90°, unit-cell volume V = 2659.05 Å3, Z = 4, and space-group P212121]. No detectable impurity was observed.

Keywords

X-ray powder diffractionDCTcefmetazoleintermediate
Type
New Diffraction Data
Information
Powder Diffraction , Volume 30 , Issue 3 , September 2015 , pp. 286 - 288
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Copyright
Copyright © International Centre for Diffraction Data 2015 

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References

Li, S. S., Wu, X. Q., Pan, Q. Q., Cheng, Q., and Li, H. (2014). “Comparison of the accuracy of powder and single crystal X-ray diffraction techniques in determining organic crystal structure,” Chin. Sci. Bull. 59, 497–501.CrossRefGoogle Scholar
Neumann, M. A. (2003). “X-cell: a novel indexing algorithm for routine tasks and difficult cases,” J. Appl. Crystallogr. 36, 356–365.CrossRefGoogle Scholar
Tang, S. Y., Zhang, Y., and Zhang, F. X. (2014). “Method of synthesis and purification of cefmetazole sodium, “Faming Zhuanli Shenqing, CN 103709179 A 20140409.Google Scholar
Wu, X. Q., Tang, P. X., Li, S. S., Zhang, L. L., and Li, H. (2014). “X-ray powder diffraction data for meloxicam, C14H13N3O4S2 ,” Powder Diffr. 29, 196–198.CrossRefGoogle Scholar
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