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X-ray powder diffraction analysis of a nonlinear optical material 3-nitro–4-hydroxy–4′-bromobenzophenone

Published online by Cambridge University Press:  10 January 2013

Zong-ming Jin ,
Zheng Jin  and
Xiang-yin Zhou
Zong-ming Jin
Affiliation:
Central Laboratory, Suzhou University, 1 Shizi Street, Suzhou, 215006, People's Republic of China
Zheng Jin
Affiliation:
Suzhou Testing Institute of Technology, 5 Minzhi Road, Suzhou, 215006, People's Republic of China
Xiang-yin Zhou
Affiliation:
Department of Chemistry, Suzhou University, 1 Shizi Street, Suzhou, 215006, People's Republic of China
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Abstract

A nonlinear optical material 3-nitro–4-hydroxy–4′-bromobenzophenone has been characterized by x-ray powder diffraction. Experimental values of 2θ, corrected for systematic errors, relative peak intensities, values of d, and the Miller indices of 109 observed reflection with 2θ up to 90° are reported. The powder diffraction data have been evaluated, and the figures-of-merit are reported. The unit cell parameters least-squares refined from 34 nonoverlapping peaks of the orthorhombic compound with a P212121 space group are a = 7.619(7) Å, b = 27.651(5) Å, c = 5.650(7) Å, V = 1190.5(9) Å3, Z = 4, and Dx = 1.389 g/cm3.

Type
Research Article
Information
Powder Diffraction , Volume 10 , Issue 2 , June 1995 , pp. 117 - 119
Copyright
Copyright © Cambridge University Press 1995

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References

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