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Synthesis and crystal data for K3Nb3O6Si2O7

Published online by Cambridge University Press:  10 January 2013

S. Launay ,
P. Mahé  and
M. Quarton
S. Launay
Affiliation:
Laboratoire de Cristallochimie du Solide, CNRS-URA 1388Université P. et M. Curie, 4 Place Jussieu, 75252 Paris Cedex 05, France
P. Mahé
Affiliation:
Laboratoire de Cristallochimie du Solide, CNRS-URA 1388Université P. et M. Curie, 4 Place Jussieu, 75252 Paris Cedex 05, France
M. Quarton
Affiliation:
Laboratoire de Cristallochimie du Solide, CNRS-URA 1388Université P. et M. Curie, 4 Place Jussieu, 75252 Paris Cedex 05, France
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Abstract

The silicate compound, K3Nb3O6Si2O7, has been synthesized by solid-state reaction. Single crystals were obtained; they crystallized with the hexagonal space group P2c. Refined unit-cell parameters are: a = 9.0377(3), c=8.0465(7)Å, V=569.18(5)Å3, Z=2, Dm = 3.84(4), Dx=3.851. Powder diffraction data are reported.

Type
Research Article
Information
Powder Diffraction , Volume 9 , Issue 2 , June 1994 , pp. 96 - 97
Copyright
Copyright © Cambridge University Press 1994

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References

Choisnet, J., Nguyen, N., Groult, D., and Raveau, B. (1976). Mat. Res. Bull. 11, 887–894.CrossRefGoogle Scholar
Mighell, A. D., Hubbard, C. R., and Stalick, J. K. (1981). NBS*AIDS 80. A FORTRAN Program for Crystallographic Data Evaluation (National Bureau of Standards, Gaithersberg, MD), Tech. Note 1141 (NBS*AIDS 83 is an expanded version of NBS*AIDS 80).CrossRefGoogle Scholar
Pagnoux, C., Guyomard, D., Verbaere, A., Piffard, Y., and Tournoux, M. (1991). C. R. Acad. Sci. Paris 312, Ser. II, 611–615.Google Scholar
Pagnoux, C., Verbaere, A., Piffard, Y., and Tournoux, M. (1993). Eur. J. Solid State Inorg. Chem. 30, 111–123.Google Scholar
Pagnoux, C. (1993). Thèse de Doctorat, Université de Nantes.Google Scholar
Shannon, R. D. (1976). Acta Cryst., A 32, 751–767.CrossRefGoogle Scholar
Smith, G. J., and Snyder, R. L. (1979). J. Appl. Crystallog. 12, 60–65.CrossRefGoogle Scholar
Stucky, G. D., Phillips, M. L. R., and Gier, T. E. (1989). Chem. Mater. 1, 492–509.CrossRefGoogle Scholar