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Synthesis and cell refinement of Ba0.5+x/2Zr2P3−xSixO12 with x=0 and 0.175

Published online by Cambridge University Press:  10 January 2013

Shanmugham Subramaniam ,
David P. Stinton ,
O. Burl Cavin ,
Camden R. Hubbard ,
Paul F. Becher  and
Santosh Y. Limaye
Shanmugham Subramaniam
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
David P. Stinton
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
O. Burl Cavin
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
Camden R. Hubbard
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
Paul F. Becher
Affiliation:
Metals and Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
Santosh Y. Limaye
Affiliation:
LoTEC. Inc., 1840 W. Parkway Boulevard, West Valley City, Utah 84119
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Abstract

Ba0.5+x/2Zr2P3−xSixO12 or BaZPS compounds were synthesized by the sintering of powders formed by a solid-state reaction. The cell parameters of Ba0.5Zr2P3O12 and Ba0.5875Zr2P2.825Si0.175O12 were determined from X-ray diffraction (XRD) data based on the (#148) space group with hexagonal setting. The cell parameters were found to increase with increasing Si content in BaZPS.

Type
Research Article
Information
Powder Diffraction , Volume 9 , Issue 2 , June 1994 , pp. 111 - 114
Copyright
Copyright © Cambridge University Press 1994

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