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Crystal data of the low-temperature solid form of 2-methyl-2-nitro-propanol(MNP)

Published online by Cambridge University Press:  10 January 2013

J. Ll. Tamarit ,
N. B. Chanh ,
P. Négrier ,
D. O. López ,
M. Barrio  and
Y. Haget
J. Ll. Tamarit
Affiliation:
Departament de Física i Enginyeria Nuclear, Universitat Politècnica de Catalunya, Diagonal, 647 08028 Barcelona, Spain
N. B. Chanh
Affiliation:
Laboratoire de Cristallographie et de Physique Cristalline URA 144 auCNRS Université Bordeaux I, 351 cours de la Libération 33405 Talence, Cedex, France
P. Négrier
Affiliation:
Laboratoire de Cristallographie et de Physique Cristalline URA 144 auCNRS Université Bordeaux I, 351 cours de la Libération 33405 Talence, Cedex, France
D. O. López
Affiliation:
Departament de Física i Enginyeria Nuclear, Universitat Politècnica de Catalunya, Diagonal, 647 08028 Barcelona, Spain
M. Barrio
Affiliation:
Departament de Física i Enginyeria Nuclear, Universitat Politècnica de Catalunya, Diagonal, 647 08028 Barcelona, Spain
Y. Haget
Affiliation:
Laboratoire de Cristallographie et de Physique Cristalline URA 144 auCNRS Université Bordeaux I, 351 cours de la Libération 33405 Talence, Cedex, France
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Abstract

By means of X-ray single crystal Weissenberg photographs, the crystal of the low-temperature solid form of 2-methyl-2-nitro-propanol, (CH3)2C(NO2)(CH2OH), has been determined and found to be of the monoclinic type, space group P21/c. The cell constants were refined from X-ray powder diffraction data: a=6.195(3) Å, b=19.116(7) Å, c=16.598(7) Å, and β = 90.12(2)° with Z = 12. The indexed pattern at 293 K is given.

Type
Research Article
Information
Powder Diffraction , Volume 9 , Issue 2 , June 1994 , pp. 84 - 86
Copyright
Copyright © Cambridge University Press 1994

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