Hostname: page-component-78c5997874-g7gxr Total loading time: 0 Render date: 2024-11-02T21:39:48.315Z Has data issue: false hasContentIssue false
  • English
  • Français

Crystal data of Nitrofurantoin C8H6N4O5

Published online by Cambridge University Press:  10 January 2013

G. Bandoli ,
A. Ongaro ,
F. Lotto  and
M. Rossi
G. Bandoli
Affiliation:
Department of Pharmaceutical Sciences, Padua University, Italy
A. Ongaro
Affiliation:
Department of Pharmaceutical Sciences, Padua University, Italy
F. Lotto
Affiliation:
FIS SpA, Alte di Montecchio Maggiore (VI), Italy
M. Rossi
Affiliation:
FIS SpA, Alte di Montecchio Maggiore (VI), Italy
Get access Rights & Permissions [Opens in a new window]

Abstract

X-ray powder diffraction of Nitrofurantoin C8H6N4O5 reveals that the compound crystallizes in a monoclinic unit cell with the powder data unit cell parameters of a = 7.852(2), b= 6.497(1), c = 18.927(5) Å, β=93.15(2)°, V=964.1(2) Å3. The unit cell dimensions determined by single crystal agree very well with those of powder diffraction analysis. A comparison with the Powder Diffraction File (PDF) 34-1603 indicates that the present data provide a more precise match to the unit cell, include additional weak reflections, along with the indexing of the powder pattern.

Type
Research Article
Information
Powder Diffraction , Volume 8 , Issue 2 , June 1993 , pp. 107 - 108
Copyright
Copyright © Cambridge University Press 1993

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Appleman, D. E., and Evans, H. T. Jr (1973). Report PB216188, U.S. Dept. of Commerce, National Technical Information Service, 5825 Port Royal Rd., Springfield, VA 22151, U.S.A.Google Scholar
Bandoli, G., Nicolini, M., and Ongaro, A. (1991). Powder Diff. 6, 196–199.CrossRefGoogle Scholar
Bandoli, G. (1992). Unpublished results.Google Scholar
Cadwallader, D. E. and Jun, H. W. (1976). Analytical Profiles Of Drug Substances, edited by Florey, K. (Academic, New York), Vol. 5, pp. 345–373.Google Scholar
Hubbard, C. R. (1982). “Standard Reference Material 640a, Si powder,” J. Appl. Crystallogr. 16, 285.CrossRefGoogle Scholar
Powder Diffraction File (1989). Pattern 34-1603. International Centre for Diffraction Data. Swarthmore, PA.Google Scholar
Robinson, W., and Sheldrick, G. M. (1988). In Crystallographic Computing 4, edited by Isaacs, N. W. & Taylor, M. R. (Oxford U.P., New York), pp. 366–377.Google Scholar
Smith, G. S., and Snyder, R. J. (1979). J. Appl. Crystallogr. 12, 60–65.CrossRefGoogle Scholar