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Published online by Cambridge University Press: 10 January 2013
Two structurally related compounds, Tl3Li(MoO4)2 and Tl3Li(WO4)2, have been synthesized by solid state reaction. Space group (P63mc) and unit-cell parameters [a(Å)=6.00392(3); c(Å)=15.8203(1) and a(Å)=6.03484(3); c(Å)=15.81759(9), respectively, for Tl3Li(MoO4)2 and Tl3Li(WO4)2] were determined. Powder diffraction data for each phase are reported.