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An alternative neutron diffractometer performance for strain/stress measurements

Published online by Cambridge University Press:  28 May 2020

Pavol Mikula*
Affiliation:
Neutron Physics Department, Nuclear Physics Institute Czech Academy of Sciences, Rez, Czech Republic
Jan Saroun
Affiliation:
Neutron Physics Department, Nuclear Physics Institute Czech Academy of Sciences, Rez, Czech Republic
Vasyl Ryukhtin
Affiliation:
Neutron Physics Department, Nuclear Physics Institute Czech Academy of Sciences, Rez, Czech Republic
James Stammers
Affiliation:
Neutron Physics Department, Nuclear Physics Institute Czech Academy of Sciences, Rez, Czech Republic
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]

Abstract

An alternative neutron diffractometer performance, which documents the feasibility of using a high-resolution three-axis neutron diffractometer for elastic and plastic deformation studies of bulk metallic polycrystalline samples, is presented. Contrary to the conventional double-axis setting, the suggested alternative consists of an unconventional three-axis set-up employing a bent perfect crystal monochromator and an analyzer with a polycrystalline sample in between. Though the alternative is, for measurements, much more time-consuming, its sensitivity to the change of the diffraction angle of the sample is, however, substantially higher and permits also plastic deformation studies on the basis of analysis of the diffraction line profiles. Moreover, much larger widths (up to 10 mm) of the irradiated gauge volumes can be investigated when just slightly affecting the angular resolution properties of the experimental setting.

Type
Technical Article
Copyright
Copyright © 2020 International Centre for Diffraction Data

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References

Davydov, V., Lukáš, P., Strunz, P., and Kužel, R. (2008). “Single-line diffraction profile analysis method used for evaluation of microstructural parameters in the plain ferritic steel upon tensile straining,” Mater. Sci. Forum 571–572, 181188.CrossRefGoogle Scholar
Delhez, R., de Keijser, T. H., and Mittemeijer, E. J. (1982). “Determination of crystallite size and lattice distortions through X-ray diffraction line profile analysis,” Fresenius’ Z. Anal. Chem. 312(1), 116.CrossRefGoogle Scholar
Hirschi, K., Ceretti, M., Lukáš, P., Ji, N., Braham, C., and Lodini, A. (1999). “Microstrain measurement in plastically deformed austenitic steel,” Textures Microstruct. 33, 219230.CrossRefGoogle Scholar
Hutchings, M. T. and Krawitz, A. D. (Eds.) (1992). Measurement of Residual and Applied Stress Using Neutron Diffraction. NATO ASI Series, Vol. 216 (Kluwer Academic Publisher, Dordrecht).CrossRefGoogle Scholar
Macek, K., Lukáš, P., Janovec, J., Mikula, P., Strunz, P., Vrána, M., and Zaffagnini, M. (1996). “Austenite content and dislocation density in electron beam welds of a stainless maraging steel,” Mater. Sci. Eng. A 208, 131138.CrossRefGoogle Scholar
Mikula, P., Vrána, M., Lukáš, P., Šaroun, J., and Wagner, V. (1996). “High-resolution neutron powder diffractometry on samples of small dimensions,” Mater. Sci. Forum 228-231, 269274.CrossRefGoogle Scholar
Mikula, P., Vrána, M., Lukáš, P., Šaroun, J., Strunz, P., Ullrich, H. J., and Wagner, V. (1997). “Neutron diffractometer exploiting Bragg diffraction optics – a high resolution strain scanner,” in Proceedings of ICRS-5, Vol. 2, edited by T. Ericsson, M. Odén and A. Andersson, June 16–18, 1997 (Linköping), pp. 721–725.Google Scholar
Noyan, I. V. and Cohen, J. B. (1987). Residual Stress: Measurement by Diffraction and Interpretation (Springer-Verlag, New York), 1st ed.CrossRefGoogle Scholar
Seong, B. S., Em, V., Mikula, P., Šaroun, J., and Kang, M. H. (2011). “Unconventional performance of a highly luminous strain/stress scanner for high resolution studies,” Mater. Sci. Forum 681, 426430.CrossRefGoogle Scholar
Stelmukh, V., Edwards, L., Santisteban, J. R., Ganguly, S., and Fitzpatrick, M. E. (2002). “Weld stress mapping using neutron and synchrotron x-ray diffraction,” Mater. Sci. Forum 404–407, 599604.CrossRefGoogle Scholar
Vrána, M., Lukáš, P., Mikula, P., and Kulda, J. (1994). “Bragg diffraction optics in high resolution strain measurements,” Nucl. Instrum. Methods Phys. Res., Sect. A 338, 125131.CrossRefGoogle Scholar