Hostname: page-component-586b7cd67f-dlnhk Total loading time: 0 Render date: 2024-11-28T10:20:42.040Z Has data issue: false hasContentIssue false
  • English
  • Français

Powder diffraction data for ferrous gluconate

Published online by Cambridge University Press:  08 December 2016

Joel W. Reid
Joel W. Reid*
Affiliation:
Canadian Light Source, 44 Innovation Boulevard, Saskatoon, SK, S7N 2V3, Canada
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]
Get access Rights & Permissions [Opens in a new window]

Abstract

Synchrotron powder diffraction data have been obtained and indexed for ferrous gluconate, a common supplement used for the treatment and prevention of iron-deficiency anemia. Ferrous gluconate (Fe(C6H11O7)2 · x H2O, Z = 4) crystallizes in a monoclinic cell (space group I2, #5) with lattice parameters a = 19.953 16(9) Å, b = 5.513 92(3) Å, c = 18.470 58(9) Å, and β = 111.3826(3)°. The pattern shows no evidence of impurity reflections.

Keywords

ferrous gluconateiron (II) gluconatesynchrotronpowder diffraction
Type
New Diffraction Data
Information
Powder Diffraction , Volume 32 , Issue 1 , March 2017 , pp. 43 - 45
Check for updates
Copyright
Copyright © International Centre for Diffraction Data 2016 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Altomare, A., Cuocci, C., Giacovazzo, C., Moliterni, A., Rizzi, R., Corriero, N., and Falcicchio, A. (2013). “EXPO2013: a kit of tools for phasing crystal structures from powder data,” J. Appl. Crystallogr. 46, 1231–1235.CrossRefGoogle Scholar
Boultif, A. and Louer, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724–731.CrossRefGoogle Scholar
Camaschella, C. (2015). “Iron-deficiency anemia,” N. Engl. J. Med. 372, 1832–1843.Google Scholar
Coe, E. M., Bowen, L. H., and Bereman, R. B. (1995). “A Mössbauer and X-ray powder diffraction study of some ferrous hematinics,” J. Inorg. Biochem. 58, 291–296.Google Scholar
Fodje, M., Grochulski, P., Janzen, K., Labiuk, S., Gorin, J., and Berg, R. (2014). “08B1-1: an automated beamline for macromolecular crystallography experiments at the Canadian light source,” J. Synchrotron Rad. 21, 633–637.Google Scholar
Groom, C. R., Bruno, I. J., Lightfoot, M. P., and Ward, S. C. (2016). “The Cambridge structural database,” Acta Crystallogr. B 72, 171–179.Google Scholar
ICDD (2015). PDF-4+ 2015 (Database), edited by Dr. Soorya Kabekkodu, International Centre for Diffraction Data, Newtown Square, PA, USA.Google Scholar
Kulgawczuk, D. S., Ruebenbauer, K., and Sepiol, B. (1989). “Mössbauer and thermogravimetric study of ferrous gluconate,” J. Radioanalyt. Nucl. Chem. 131, 43–50.Google Scholar
Le Bail, A. (2004). “Monte carlo indexing with mcmaille,” Powder Diffr. 19, 249–254.Google Scholar
Le Bail, A., Duroy, H., and Fourquet, J. L. (1988). “Ab-initio structure determination of LiSbWO6 by X-ray powder diffraction,” Mater. Res. Bull. 23, 447–452.Google Scholar
Pizarro, F., Boccio, J., Salgueiro, M., Olivares, M., Carmuega, E., Weill, R., Marque, S., Frereux, M., and Noirt, F. (2013). “Bioavailability of stabilised ferrous gluconate with glycine in fresh cheese matrix: a novel iron compound for food fortification,” Biol. Trace Elem. Res. 151, 441–445.Google Scholar
Radtke, H., Tegtmeier, J., Rӧcker, L., Salama, A., and Kiesewetter, H. (2005). “Compensating for iron loss in regular blood donors using ferrous gluconate and ascorbic acid,” Transfusion 45, 1236–1237.CrossRefGoogle ScholarPubMed
Reznikoff, P. and Goebel, W. F. (1937). “The use of ferrous gluconate in the treatment of hypochromic anemia,” J. Clinic. Invest. 16, 547–554.CrossRefGoogle ScholarPubMed
Rodriguez-Carvajal, J. (2001). “Recent developments of the program FULLPROF,” IUCR Newslett. 26, 12–19.Google Scholar
Toby, B. H. and Von Dreele, R. B. (2013). “GSAS II: the genesis of a modern open-source all-purpose crystallography software package,” J. Appl. Crystallogr. 46, 544–549.CrossRefGoogle Scholar
Villalpando, S., Shamah, T., Rivera, J. A., Lara, Y., and Monterrubio, E. (2006). “Fortifying milk with ferrous gluconate and zinc oxide in a public nutrition program reduced the prevalence of anemia in toddlers,” J. Nutr. 136, 2633–2637.Google Scholar
Supplementary material: File

Reid supplementary material

Reid supplementary material 1

Download Reid supplementary material(File)
File 70.1 KB