Hostname: page-component-586b7cd67f-l7hp2 Total loading time: 0 Render date: 2024-11-24T15:59:38.997Z Has data issue: false hasContentIssue false

Synthesis of FeAl Hetero-Nanostructured Bulk Parts via Spark Plasma Sintering of Milled Powder

Published online by Cambridge University Press:  26 February 2011

Thierry Grosdidier
Affiliation:
[email protected], Laboratoire d'Etude des Textures et Application aux Matériaux (LETAM), UMR CNRS 7078, Université de Metz, Ile du Saulcy, Metz, 57045, France
Gang Ji
Affiliation:
[email protected], Laboratoire d'Etude des Textures et Application aux Matériaux (LETAM), UMR CNRS 7078, Université de Metz, Ile du Saulcy, Metz, 57045, France
Frédéric Bernard
Affiliation:
[email protected], Laboratoire de Recherche sur la Réactivité des Solides (LRRS), UMR CNRS 5613, Université de Bourgogne, 9 avenue Alain Savary, Dijon, 21078, France
Sébastien Launois
Affiliation:
[email protected], Département des Technologies des Nanomatériaux, Commissariat à l'Energie Atomique, 17 rue des Martyrs, Grenoble, 38054, France
Get access

Abstract

Spark plasma sintering (SPS) has been used in order to introduce nanocrystalline grains within fully dense FeAl consolidated parts. Hetero-nanostructured parts, consisting of nano, ultrafine and micrometric grains, have been successfully processed when milled - Y2O3 reinforced - FeAl powder was used. The large temperature differences that are spontaneously generated during the SPS process as well as the use of milled powder account for the formation of such interesting structures. The grain size distribution - that is suggested to be very potent to improve both strength and ductility - could be significantly modified by a proper selection of sintering temperature and holding time.

Type
Research Article
Copyright
Copyright © Materials Research Society 2007

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Moret, F., Baccino, R., Martel, P. and Guetaz, L., J. Phys. IV 6, 281(1996).Google Scholar
2. Revol, S., Launois, S., Baccino, R., Sire, P., Girard, Y. and Sereni, S., Proceedings of PM Conference EURO PM2001, European Conference on Powder Metallurgy, Nice, France, 22–24 October 2001. pp. 20012003.Google Scholar
3. Takasugi, T., Masahashi, N. and Izumi, O., Acta Metall. 35, 381(1987).Google Scholar
4. Deevi, S.C. and Sikka, V.K., Intermetallics 4, 357(1996).Google Scholar
5. Baker, I. and Munroe, P.R., Inter. Mater. Rev. 42, 181(1997).Google Scholar
6. Stoloff, N.S., Mater. Sci. Eng. A258, 1(1998).Google Scholar
7. Gaydosh, D.J., Draper, S.L., Noebe, R.D. and Nathal, M.V., Mater. Sci. Eng. A150, 7(1992).Google Scholar
8. Morris, D.G. and Gunther, S., Mater. Sci. Eng. A208, 7(1996).Google Scholar
9. Baccino, R., Wolski, K., Thevenot, F., Lecoze, J. and Moret, F., Ann. Chim. Sci. Mat. 22, 423(1997).Google Scholar
10. Schneibel, J.H., George, E.P. and Anderson, I.M., Intermetallics 5, 185(1997).Google Scholar
11. Subramanian, R. and Schneibel, J.H., Acta Mater. 46, 4733(1998).Google Scholar
12. Grosdidier, T., Suzon, E. and Wagner, F., Intermetallics 12, 645(2004).Google Scholar
13. Morris, D.G., Muñoz-Morris, M.A. and Chao, J., Intermetallics 12, 821(2004).Google Scholar
14. Omori, M., Mater. Sci. Eng. A287, 183(2000).Google Scholar
15. Tokita, M., Mater. Sci. Forum 423, 39(2003).Google Scholar
16. Minamino, Y., Koizumi, Y., Tsuji, N., Hirohata, N., Mizuuchi, K. and Ohkanda, Y., Sci. Techn. Adv. Mater. 5, 133(2004).Google Scholar
17. Lee, S.H., Moon, K.I., Hong, H.S. and Lee, K.S., Intermetallics 11, 1039(2003).Google Scholar
18. Grosdidier, T., Ji, G., Bernard, F., Gaffet, E., Munir, Z.A. and Launois, S., Intermetallics 14, 1208(2006).Google Scholar
19. Ji, G., Grosdidier, T., Bozzolo, N. and Launois, S., Intermetallics; in press.Google Scholar
20. Ji, G., Grosdidier, T., Liao, H.L., Morniroli, J.P. and Coddet, C., Intermetallics 13, 596(2005).Google Scholar
21. Grosdidier, T., Tidu, A. and Liao, H.L., Scripta Mater. 44, 387(2001).Google Scholar
22. Koch, C.C., Scripta Mater. 49, 657(2003).Google Scholar
23. Ma, E., Scripta Mater. 49, 663(2003).Google Scholar