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Solid State NMR Studies of Lead(II) Thiourea Materials

Published online by Cambridge University Press:  26 February 2011

Cecil Dybowski ,
Alicia Glatfelter ,
Shi Bai ,
D. Martinez ,
S. Segarra  and
Dale L. Perry
Cecil Dybowski
Affiliation:
[email protected] University of Delaware Department of Chemistry and Biochemistry Newark DE 19716 United States
Alicia Glatfelter
Affiliation:
[email protected] University of Delaware Department of Chemistry and Biochemistry Newark DE 19716 United States
Shi Bai
Affiliation:
[email protected] University of Delaware Department of Chemistry and Biochemistry Newark DE 19716 United States
D. Martinez
Affiliation:
[email protected] University of California Lawrence Berkeley National Laboratory MS 70A-1150 Berkeley CA 94720 United States
S. Segarra
Affiliation:
[email protected] University of California Lawrence Berkeley National Laboratory MS 70A-1150 Berkeley CA 94720 United States
Dale L. Perry
Affiliation:
[email protected] University of California Lawrence Berkeley National Laboratory MS 70A-1150 Berkeley CA 94720 United States
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Abstract

Solid-state 13C and 207Pb NMR have been used to characterize a series of lead(II) ion complexes containing thiourea – widely used in materials science – as the organic complexing molecule. NMR data for the complexes have been measured and discussed with respect to the reported structures for the complexes.

Keywords

nuclear magnetic resonance (NMR)Pbchemical synthesis
Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 984: Symposium MM – Magnetic Resonance in Material Science , 2006 , 0984-MM07-20
Copyright
Copyright © Materials Research Society 2007

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