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Nanophase Copper Ferrite Using an Organic Gelation Technique

Published online by Cambridge University Press:  10 February 2011

D. Sriram ,
R. L. Snyder  and
V. R. W. Amarakoon
D. Sriram
Affiliation:
NYS College of Ceramics, Alfred University, Alfred, NY 14802
R. L. Snyder
Affiliation:
Dept. of Materials Science and Engineering, The Ohio State University, Columbus, OH 43210
V. R. W. Amarakoon
Affiliation:
NYS College of Ceramics, Alfred University, Alfred, NY 14802
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Abstract

Nanocrystalline copper ferrite (Cu0.5Fe2.5O4) was synthesized using a forward strike gelation method with polyacrylic acid (PAA) as a gelating agent. The dried gel was calcined at a low temperature of 400 °C to get the final powder. The effect of pH and the ratio of the cation to the carboxylic group in the initial gel were studied with respect to both the phases and the crystallite size of the final powders synthesized. Phase and crystallite size analysis were done using x-ray diffraction and TEM. Saturation magnetization results were obtained using a SQUID magnetometer. The reactions occurring in the nano-size copper ferrite, in air as a function of temperature, were tracked using adynamic high temperature x-ray diffraction (HTXRD) system.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 457: Symposium V – Nanophase and Nanocomposite Materials II , 1996 , 81
Copyright
Copyright © Materials Research Society 1997

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References

REFERENCES

1. Micheli, A.L., U.S. Patent No. 4,627,966 (9 December 1986).Google Scholar
2. McCluskey, P. H., Snyder, R. L. and Condrate, R. A. Sr, J. Solid State Chem., 83 (2), 332–339 (1989).Google Scholar
3. McCluskey, P. H., Fischman, G. S. and Snyder, R. L., J. Therm. Anal., 34 (5–6), 1441–1448 (1988).Google Scholar
4. Fagan, J.F., PhD thesis, Alfred University, 1995.Google Scholar
5. Nagarajan, A., and Agajanian, A.H., J. Appl. Phys., 41 (4), 1642–1647 (1969).Google Scholar
6. Sriram, D. and Snyder, R.L., Symp. Proc. Series, Mat. Res. Soc., 401, 180–185 (1995)Google Scholar
7. Howard, S. A. and Snyder, R. L., J. Appl. Crystallogr., 22, 238–243 (1989).Google Scholar
8. Chen, B. J., Rodriguez, M. A., Misture, S. T. and Snyder, R. L., Physica C, 195, 118–124 (1992).Google Scholar
9. Snyder, R. L., Advanced Materials & Processes, 8/94, 20–25 (1994).Google Scholar