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Published online by Cambridge University Press: 10 February 2011
An ultra high vacuum (UHV) deposition/bonding system has been constructed that can produce planar interfaces from a wide array of materials. The interfaces in this system can be synthesized in-situ by UHV diffusion bonding of two substrates with or without various interfacial layers. Substrate surfaces can be heat treated, sputter cleaned and characterized in-situ prior to deposition and/or bonding. Interfacial layers can be deposited by e-beam evaporation and/or sputter deposition in any layered or alloyed combination. After deposition, the two substrates are bonded in UHV, by the application of heat and pressure.
This synthesis procedure permits systematic variation and control of interface morphology and chemistry. Integrity of the bonded interface as well as the microstructure and chemistry are examined by cross-sectional analytical transmission electron microscopy. In this study, stainless steel and single and polycrystalline alumina were used as substrate materials to produce interfaces with and without Ti and Cu interlayers.