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Bimetallic Alloy of Fe2O3-Ag Nanoparticles: Characterization and Structural Modeling

Published online by Cambridge University Press:  22 July 2016

A. Ruíz-Baltazar ,
R. Esparza ,
J.L López-Miranda ,
G. Rosas  and
R. Pérez
A. Ruíz-Baltazar*
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001,76230 Santiago de Querétaro, QRO, México.
R. Esparza
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001,76230 Santiago de Querétaro, QRO, México.
J.L López-Miranda
Affiliation:
Instituto de Investigaciones Metalúrgicas, Universidad Michoacana, C.U. C.P: 77000, Morelia, México.
G. Rosas
Affiliation:
Instituto de Investigaciones Metalúrgicas, Universidad Michoacana, C.U. C.P: 77000, Morelia, México.
R. Pérez
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001,76230 Santiago de Querétaro, QRO, México.
*
*Email: [email protected]
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Abstract

The synthesis of Fe3O4-Ag bimetallic nanoparticles by chemical reduction was carried out. Fe nanoparticles were obtained using Fe (III) Chloride hexahydrate (FeCl3•6H2O) as precursor and sodium borohydride (NaBH4) as reducing agent, subsequently, a solution of silver nitrate (AgNO3) was added to the reaction. The synthesis methodology employed in this case, is a modification of chemical reduction method. Through this procedure has been possible simplify the synthesis route used to obtain bimetallic systems such as Fe3O4-Ag. Particles with semi-spherical morphology were observed. High-resolution transmission electron microscopy (HREM), ultraviolet visible spectroscopy (UV-is) and quasi-elastic light scattering (QELS) techniques were employed for the structural characterization of Fe3O4-Ag nanostructures. Some models presented describe and prove the formation of the Fe3O4-Ag alloy type structures.

Keywords

Chemical synthesisSEMNanostructure
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1816: Symposium 5B – Structural and Chemical Characterization of Metals, Alloys and Compounds , 2016 , imrc2015absp1
Copyright
Copyright © Materials Research Society 2016 

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References

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