Hostname: page-component-586b7cd67f-2brh9 Total loading time: 0 Render date: 2024-11-28T13:17:51.909Z Has data issue: false hasContentIssue false
  • English
  • Français

Microstructure and Mechanical Properties Characterisation of Nanocrystalline Copper Films

Published online by Cambridge University Press:  01 February 2011

Nursiani Indah Tjahyono  and
Yu Lung Chiu
Nursiani Indah Tjahyono
Affiliation:
[email protected], University of Auckland, Department of Chemical and Materials Engineering, 20 Symonds Street, Auckland, 1142, New Zealand
Yu Lung Chiu
Affiliation:
[email protected], University of Auckland, Department of Chemical and Materials Engineering, 20 Symonds Street, Auckland, 1142, New Zealand
Get access

Abstract

The microstructure and mechanical properties of nanocrystalline copper with grain size ranging from 50 nm to 80 nm have been investigated. Thin films of nanocrystalline copper were electrodeposited from an additive-free acidified copper sulphate solution at room temperature by employing constant current at different current density magnitudes between 20 and 80 mA/cm2. Both austenitic and ferritic steel substrates with the same surface finishing conditions have been used for the deposition. The microstructure of the thin films has been further studied using electron microscopy techniques, and the mechanical properties using nanoindentation technique. The nanoindentation study was carried out on both the plan view and cross-sectional directions to study the isotropy characteristic of the copper film. It has been noted that both the modulus and hardness measured following the Oliver-Pharr scheme show an apparent indentation size effect tested on the cross-sectional sample.

Keywords

Cumicrostructurehardness
Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 1049: Symposium AA – Fundamentals of Nanoindentation and Nanotribology IV , 2007 , 1049-AA03-05
Copyright
Copyright © Materials Research Society 2008

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1 Al-Rub, A. and Rashid, K., Mech. Mater. 39, 787 (2007).Google Scholar
2 Seah, C.H., Mridha, S., and Chan, L.H., J. Mater. Proc. Technol. 89–90, 432 (1999).Google Scholar
3 “Nanostructured Coatings”, edited by. Cavaleiro, A. and Hosson, J.T.M.D., Springer, New York (2006).Google Scholar
4 Choi, Y., Vliet, K.J. Van, Li, J., and Suresh, S., J. Appl. Phys. 94,6050 (2003).Google Scholar
5 Tao, S. and Li, D.Y., Nanotechnology. 17, 65 (2006).Google Scholar
6 Fang, T.H. and Chang, W.J., Microelect. Eng. 65, 231 (2003).Google Scholar
7 Beegan, D., Chowdhury, S., and Laugier, M.T., Surf. Coat. Technol. 176, 124 (2003).Google Scholar
8 Volinsky, A.A., Vella, J., Adhihetty, I.S., Sarihan, V., Mercado, L., Yeung, B.H., and Gerberich, W.W.. in Fundamentals of Nanoindentation and Nanotribology II, edited by Baker, S. P., Cook, R. F., Corcoran, S. G., and Moody, N. R. (Mater. Res. Soc. Symp. Proc. 649, Boston, MA, 2000) pp. Q.5.3.1–5.3.6.Google Scholar
9 Chan, C.Y., Zhang, W.J., Matsumoto, S., Bello, I., Lee, S.T., J. Crystal Growth, 247, 438 (2003).Google Scholar
10 Chen, X. and Vlassak, J.J.. in Fundamentals of Nanoindentation and Nanotribology II, edited by Baker, S. P., Cook, R. F., Corcoran, S. G., and Moody, N. R. (Mater. Res. Soc. Symp. Proc. 649, Boston, MA, 2000) pp. Q.1.3.1–1.3.6.Google Scholar
11 Feng, G. and Nix, W.D., Scripta Mater. 51, 599 (2004).Google Scholar
12 Manika, I. and Maniks, J., Acta Mater. 54, 2049 (2006).Google Scholar
13 Zhao, M., Slaughter, W.S., Li, M., Mao, S.X., Acta Mater. 51, 4461 (2003).Google Scholar
14 Mukhopadhyay, N.K. and Paufler, P., Inter. Mater. Rev. 51, 209 (2006).Google Scholar
15 Schiøtz, J., Tolla, F.D. Di and Jacobsen, K.W., Nature 391 (1998).Google Scholar