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Influence of Grain Orientation on the Microstructural Characterization in Cu During (self)-Anneal using a Surface Acoustic wave Technique

Published online by Cambridge University Press:  01 February 2011

Atsuko Sekiguchi
Affiliation:
[email protected], Imec, SPDT/ITTO, Kapeldreef 75, Leuven, N/A, N/A, Belgium
Kris Vanstreels
Affiliation:
[email protected], IMO/Hasselt University, Diepenbeek, N/A, 3590, Belgium
Steven DeMuynck
Affiliation:
[email protected], Imec, Leuven, N/A, 3001, Belgium
Jan D'Haen
Affiliation:
[email protected], IMO/Hasselt University, Diepenbeek, N/A, 3590, Belgium
Sywert H Brongersma
Affiliation:
[email protected], Imec, Leuven, N/A, 3001, Belgium
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Abstract

This paper describes the influence of microstructure, or more specifically grain orientation and grain size, on the in-line monitoring of copper interconnect properties during (self)-anneal using surface acoustic wave spectroscopy (SAWS). In electroplated Cu after (self)-anneal the SAWS frequency is lower for samples annealed at higher temperature because of the lower porosity induced elasticity. In sputtered Cu, the SAWS frequency shows a clear correlation with grain size, which is induced by a strong re-orientation of the copper film from the as-deposited (111) texture (E=190 GPa) to a strongly (100) textured super grain structure (E=78GPa).

Type
Research Article
Copyright
Copyright © Materials Research Society 2006

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References

1 Duggal, A.R., Rogers, J.A., Nelson, K.A., J. Appl. Phys. 72, 2823 (1992).Google Scholar
2 Dhar, L., Rogers, J.A., Nelson, K.A. and Trusell, F., J. Appl. Phys. 77, 4431 (1995).Google Scholar
3 Sekiguchi, A., presented at the 2006 MAM conference, Grenoble, France, 2006 (unpunlished).Google Scholar
4 Sanders, P.G., Eastman, J.A. and Weertman, J.R., Acta. Mater. 45, 4019 (1997).Google Scholar
5 Huang, H. and Spaepen, F., Acta Mater. 48, 3261 (2000).Google Scholar
6 Shen, T.D., Koch, C.C., Tsui, T.Y. and Pharr, G.M., J. Mater. Res. 10, 2892 (1995).Google Scholar
7 , Spriggs, J. Am. Ceram. 44, 70 (1961)Google Scholar
8 Hommel, M. and , Kraft, Acta. Mater. 49, 3935 (2001).Google Scholar
9 Uedono, A., Suzuki, T. and Nakamura, T., J. Appl. Phys. 98, 043504(2005).Google Scholar