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Synthesis of magnesium hydroxide nanoneedles and short nanorods on polymer dispersant template

Published online by Cambridge University Press:  31 January 2011

Hong Yan
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology, Ministry of Education, Taiyuan, Shanxi 030024, People’s Republic of China; and College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 030024, People’s Republic of China
Jianming Wu
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology, Ministry of Education, Taiyuan, Shanxi 030024, People’s Republic of China; and College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 030024, People’s Republic of China
Xuehu Zhang
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology, Ministry of Education, Taiyuan, Shanxi 030024, People’s Republic of China; and College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 030024, People’s Republic of China
Yan Zhang
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology, Ministry of Education, Taiyuan, Shanxi 030024, People’s Republic of China; and College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 030024, People’s Republic of China
Liqiao Wei
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology, Ministry of Education, Taiyuan, Shanxi 030024, People’s Republic of China; and College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 030024, People’s Republic of China
Xuguang Liu
Affiliation:
College of Chemistry and Chemical Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 030024, People’s Republic of China
Bingshe Xu*
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology, Ministry of Education, Taiyuan, Shanxi 030024, People’s Republic of China; and College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan, Shanxi 030024, People’s Republic of China
*
a)Address all correspondence to this author.e-mail: [email protected]
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Abstract

Magnesium hydroxide nanoneedles and nanorods were synthesized by reverse precipitation in the presence of polyethylene glycol (MW 1000) at ambient temperature. The obtained magnesium hydroxide crystals were characterized in terms of morphology, particle size, crystal structure, and thermal stability by high-resolution transmission electron microscopy, x-ray diffraction, infrared spectroscopy, and thermogravimetric and differential thermal analysis. The experimental results show that the growth of magnesium hydroxide crystals and the dispersivity of the nanostructures were greatly influenced by polymer dispersant. The mechanism of the formation of magnesium hydroxide nanorods and nanoneedles was also proposed.

Type
Articles
Copyright
Copyright © Materials Research Society 2007

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References

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