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Sol–gel synthesis of fine-particle superconducting oxide, YBa2Cu3O7−x

Published online by Cambridge University Press:  31 January 2011

P. Ravindranathan
Affiliation:
Materials Research Laboratory, The Pennsylvania State University, University Park, Pennsylvania 16802
S. Komarneni
Affiliation:
Materials Research Laboratory, The Pennsylvania State University, University Park, Pennsylvania 16802
A. Bhalla
Affiliation:
Materials Research Laboratory, The Pennsylvania State University, University Park, Pennsylvania 16802
R. Roy
Affiliation:
Materials Research Laboratory, The Pennsylvania State University, University Park, Pennsylvania 16802
L. E. Cross
Affiliation:
Materials Research Laboratory, The Pennsylvania State University, University Park, Pennsylvania 16802
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Abstract

A sol-gel method of preparing fine-particle superconducting oxide YBa2Cu3O7−x was developed. Single-phase superconducting oxide YBa2Cu3O7−x formed at temperatures as low as 750°. The particle size obtained by this method was found to be ≤0.2μm. Pellets sintered from these sol-gel powders exhibited very sharp resistivity drops at Tc = 90 °C with a Δc of ∼3°K.

Type
Rapid Communications
Copyright
Copyright © Materials Research Society 1988

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References

REFERENCES

1Bednorz, J. and Müller, A. K., Z. Phys. B 64, 189 (1986).CrossRefGoogle Scholar
2Uchida, S., Takagi, H., Kitazawa, K., and Tanaka, S., Jpn. J. Appl. Phys. 26, L1 (1987).Google Scholar
3Wu, M. K., Ashburn, J. R., Torng, C. J., Hor, P. H., Meng, R. L., Gao, L., Huang, Z. J., Wang, Y. Q., and Chu, C. W., Phys. Rev. Lett. 58, 980 (1987).Google Scholar
4Ganguly, P., Raychaudhuri, A.K., Sreedhar, A. K., and Rao-Pramana, C. N. R., J. Phys. 27, 229 (1987).Google Scholar
5Cima, M. J. and Rhine, W. E., Adv. Ceram. Mater. 2(3B), 329 (1987).CrossRefGoogle Scholar
6Manthiram, A. and Goodenough, J. B., Nature 329, 701 (1987).Google Scholar
7Ritter, J. J., First International Conference on Ceramic Powder Processing Science, Orlando, FL, 1-4 November 1987.Google Scholar
8Barboux, P., Tarason, J. M., Bagley, B. G., Greene, L. H., and Hull, G. W., The Materials Research Society, Boston, 30 November -5 December 1987.Google Scholar
9Hoffman, D., Roy, R., and Komarneni, S., Mater. Lett. 2, 245 (1984).Google Scholar
10Roy, R., Science 238, 1664 (1987).Google Scholar
11Kijowski, A. K., Komarneni, S., and Roy, R., in Better Ceramics Through Chemistry, edited by Brinker, C. J., Clark, D. E., and Ulrich, D. R. (Mater. Res. Soc, Pittsburgh, PA, to be published), Vol. 3.Google Scholar
12Wong-Ng, W., Roth, R. S., Swartzendruber, L. J., Bennett, L. H., Chiang, C. K., Beech, F., and Hubbard, C. R., Adv. Ceram. Mat. 2 (3B), 565 (1987).Google Scholar