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Simple synthesis of polyaniline microtubes for the application on silver microrods preparation

Published online by Cambridge University Press:  05 January 2012

Youyi Sun ,
Guizhen Guo ,
Binghua Yang ,
Minhong He ,
Ye Tian ,
JianChao Cheng  and
Yaqing Liu
Youyi Sun*
Affiliation:
Research Center for Engineering Technology of Polymeric Composites of Shanxi Province, North University of China, Taiyuan 030051, People’s Republic of China; and Key Laboratory for Instrumentation Science & Dynamic Measurement, North University of China, Taiyuan 030051, People’s Republic of China
Guizhen Guo
Affiliation:
Research Center for Engineering Technology of Polymeric Composites of Shanxi Province, North University of China, Taiyuan 030051, People’s Republic of China
Binghua Yang
Affiliation:
Research Center for Engineering Technology of Polymeric Composites of Shanxi Province, North University of China, Taiyuan 030051, People’s Republic of China
Minhong He
Affiliation:
Research Center for Engineering Technology of Polymeric Composites of Shanxi Province, North University of China, Taiyuan 030051, People’s Republic of China
Ye Tian
Affiliation:
Research Center for Engineering Technology of Polymeric Composites of Shanxi Province, North University of China, Taiyuan 030051, People’s Republic of China
JianChao Cheng
Affiliation:
Research Center for Engineering Technology of Polymeric Composites of Shanxi Province, North University of China, Taiyuan 030051, People’s Republic of China
Yaqing Liu
Affiliation:
Research Center for Engineering Technology of Polymeric Composites of Shanxi Province, North University of China, Taiyuan 030051, People’s Republic of China
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

Polyaniline (PANI) microtubes were successfully synthesized by a simple way without using any templates. Their structure was characterized by scanning electron microscopy, transmission electron microscopy, x-ray diffraction, ultraviolet–visible absorption spectra, and Fourier transform infrared spectroscopy. The average length and diameter of the microtubes were about 12.0 and 3.0 μm, respectively. In addition, silver microrods were further prepared using the PANI microtubes as templates. Scanning electron microscopy, energy-dispersive x-ray spectra, x-ray diffraction, and ultraviolet–visible absorption spectra analyses were performed to characterize the structure of the sample. The results indicated the formation of silver microrods inside PANI microtubes. Moreover, the microwave absorption and electrical properties of PANI microtubes, PANI particles, and silver microrods were compared. It shows that the silver microrods coated with PANI have good microwave absorption and electrical properties, which can apply on electromagnetic interference shielding and microwave absorption materials.

Keywords

AgCompositeMicrostructure
Type
Articles
Information
Journal of Materials Research , Volume 27 , Issue 2 , 28 January 2012 , pp. 457 - 462
Copyright
Copyright © Materials Research Society 2011

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