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Reactive conversion of polycrystalline SnO2 into single-crystal nanofiber arrays at low oxygen partial pressure

Published online by Cambridge University Press:  31 January 2011

Carmen M. Carney ,
Sheikh A. Akbar ,
Ye Cai ,
Sehoon Yoo  and
Kenneth H. Sandhage
Carmen M. Carney
Affiliation:
Department of Materials Science and Engineering, The Ohio State University, Columbus, Ohio 43212
Sheikh A. Akbar*
Affiliation:
Department of Materials Science and Engineering, The Ohio State University, Columbus, Ohio 43212
Ye Cai
Affiliation:
School of Materials Science and Engineering, Georgia Institute of Technology, Atlanta, Georgia 30332
Sehoon Yoo
Affiliation:
School of Materials Science and Engineering, Georgia Institute of Technology, Atlanta, Georgia 30332
Kenneth H. Sandhage*
Affiliation:
School of Materials Science and Engineering, School of Chemistry and Biochemistry, Georgia Institute of Technology, Atlanta, Georgia 30332
*
a)Address all correspondence to these authors. e-mail: [email protected]
b)Address all correspondence to these authors. e-mail: [email protected]
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Abstract

Single-crystal SnO2 nanofibers have been formed from SnO2 polycrystals via reaction at low oxygen partial pressures. Polycrystalline SnO2 disks coated with Au nanoparticles were exposed to humid H2/N2 at 700 to 800 °C. Single-crystal SnO2 nanofibers formed beneath Au nanoparticles, with the nanofiber length oriented parallel to the [100] crystallographic direction of SnO2. Because this simple process does not require either a separate source of a Sn–O-bearing vapor species located upstream of the substrate or a temperature gradient, single-crystal nanofibers may be formed on large area SnO2-bearing substrates.

Keywords

NanostructureOxideSurface reaction
Type
Articles
Information
Journal of Materials Research , Volume 23 , Issue 10 , October 2008 , pp. 2639 - 2644
Copyright
Copyright © Materials Research Society 2008

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References

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