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Rapid constructing magnetic phase diagrams by magneto-optical imaging of composition spread films

Published online by Cambridge University Press:  03 March 2011

M.J. Turchinskaya ,
L.A Bendersky ,
A.J. Shapiro ,
K.S. Chang ,
I. Takeuchi  and
A.L. Roytburd
M.J. Turchinskaya
Affiliation:
Metallurgy Division, Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, Maryland 20899
L.A Bendersky*
Affiliation:
Metallurgy Division, Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, Maryland 20899
A.J. Shapiro
Affiliation:
Metallurgy Division, Materials Science and Engineering Laboratory, National Institute of Standards and Technology, Gaithersburg, Maryland 20899
K.S. Chang
Affiliation:
Department of Materials Science and Engineering, University of Maryland, College Park, Maryland 20742
I. Takeuchi
Affiliation:
Department of Materials Science and Engineering, University of Maryland, College Park, Maryland 20742
A.L. Roytburd
Affiliation:
Department of Materials Science and Engineering, University of Maryland, College Park, Maryland 20742
*
a) Address all correspondence to this author. e-mail: [email protected]
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Abstract

In this paper we present a new method of the rapid construction of magnetic phase diagrams in a temperature-composition space, using magneto-optic imaging with an indicator film technique (MOIF). The method is applied for mapping the diagram for the La1–xCaxMnO3 colossal magneto-resistive oxide, using the spread films deposited on a SrTiO3 substrate. The constructed magnetic diagram is in a good agreement with data on uniform films and bulk crystals of this system. The MOIF study of transitions under cooling and heating has revealed the formation of a non-magnetic phase in the area of temperatures from 5 K to 57 K and compositions from x = 0 to x = 0.5.

Keywords

Combinatorial synthesisDeposition (PLD)Magnetic properties
Type
Rapid Communications
Information
Journal of Materials Research , Volume 19 , Issue 9 , September 2004 , pp. 2546 - 2548
Copyright
Copyright © Materials Research Society 2004

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References

REFERENCES

1.Fukumura, T., Ontani, M., Kawasaki, M., Okimoto, Y., Kageyama, T., Koida, T., Hasegawa, T., Tokura, Y. andKoinuma, H.: Rapid construction on phase diagram for doped Mott insulators with a composition-spread approach. Appl. Phys. Lett. 77, 3426 (2000).CrossRefGoogle Scholar
2.Yoo, Y.K. and Tsui, F.: Continuous phase diagramming of epitaxial films. MRS Bull. 316 April (2002).Google Scholar
3.Dorosinskii, L.A., Indenbom, M.V., Nikitenko, V.I., Ossip’yan, Yu.A., Polyanskii, A.A. andVlasko-Vlasov, V.K.: Studies of HTSC crystal magnetization features using indicator magnetooptic films with in-plane anisotropy. Physica C 203, 149 (1992).CrossRefGoogle Scholar
4.Turchinskaya, M., Smith, D.T., Roytburd, A.L. andKaiser, D.L.: Vortex pinning in microindented YBa2Cu3O7-3. J. Appl. Phys. 88, 1541 (2000).CrossRefGoogle Scholar
5.Vlasko-Vlasov, K., Lin, Y.K., Miller, D.J., Welp, U., Crabtree, G.W. andNikitenko, V.I.: Direct magneto-optical observation of a structural phase transition in thin films of manganites. Phys. Rev. Lett. 84, 2239 (2000).CrossRefGoogle ScholarPubMed
6.Indenbom, M.V., Forcl, A., Ludescher, B., Kronmüller, H., Habermeier, H.U., Leibold, B., D’Anna, G., Li, T.W., Kess, P.H. andMenovsky, A.A.: Anisotropy of perpendicular field penetration into high—Tc superconductors induced by strong longitudinal field. Physica C 226, 325 (1994).CrossRefGoogle Scholar
7.Cheong, C-W. andHwang, H.Y. In Ferromagnetism vs. Charge/Orbital Ordering in Mixed–Valent Manganites: Colossal Magneto-resistive Oxides, edited by Tokura, Y. (Gordon and Breach Science Publisher, The Netherlands, Amsterdam, 2000), p. 237Google Scholar
8.Chang, K.S., Aronova, M., Famudu, O., Takeuchi, I., Lofland, S.E., Hattrick-Simpers, J. andChang, H.: Multimode quantitative scanning microwave microscopy in situ grown epitaxial Ba1-xSrxTiO3 compositional spreads. Appl. Phys. Lett. 79, 4411 (2001).CrossRefGoogle Scholar
9.Huang, Q., Lynn, J.W., Erwin, R.W., Santono, E., Dender, D.C., Smolyaninova, V.N., Ghost, K. andGreene, R.L.: Temperature and field dependence of the phase separation, structure, and magnetic ordering in La1-xCaxMnO3 (x=0.47, 0.50, and 0.53). Phys. Rev. B 61, 8895 (2000).CrossRefGoogle Scholar
10.Praus, R.B., Gross, G.M., Razavi, F.S. andHabermeier, H-U.: Effects of strain on properties of La0.67Ca0.33MnO3 thin films. J. Magn. Magn. Mater. 211, 41 (2000).CrossRefGoogle Scholar
11.Levy, F., Parisi, G., Polla, D., Vega, G., Leyva, M., Lamza, R., Freitas, S. andChivelder, L.: Controlled phase separation in La0.5Ca0.5MnO3. Phys. Rev. B 62, 6437 (2000).CrossRefGoogle Scholar
12.Mathur, N. and Littlewood, P.: Mesotopic texture in manganities. Phys. Today 25 January (2003).Google Scholar
13.Loudon, J.C., Mathur, N.D. andMidgley, P.A.: Charge-ordered ferromagnetic phase in La0.5Ca0.5MnO3. Nature 420, 797 (2002).CrossRefGoogle Scholar