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Magnetic field–dependent microstructure evolution and magnetic property of Fe–6.5 Si–0.05 B alloy during solidification

Published online by Cambridge University Press:  09 December 2019

Chunmei Liu ,
Yunbo Zhong ,
Zhe Shen ,
Licheng Dong ,
Tianxiang Zheng ,
Weili Ren ,
Zuosheng Lei  and
Zhongming Ren
Chunmei Liu
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Yunbo Zhong*
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Zhe Shen
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Licheng Dong
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Tianxiang Zheng*
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Weili Ren
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Zuosheng Lei
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
Zhongming Ren
Affiliation:
State Key Laboratory of Advanced Special Steel & Shanghai Key Laboratory of Advanced Ferrometallurgy & School of Materials Science and Engineering, Shanghai University, Shanghai 200072, China
*
a)Address all correspondence to these authors. e-mail: [email protected]
b)e-mail: [email protected]
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Abstract

Fe–6.5 Si–0.05 B alloy was used in the study to investigate the texture evolution and magnetic property of the ferromagnetic crystal under an axial high magnetic field during bulk solidification. Optical microscopy (OM) and X-ray diffraction (XRD) were applied to analyze the microstructures and texture evolution of the alloy solidified under different magnetic field intensities. The result shows that with an increase in the magnetic field intensity from 0 to 2 T, the texture gradually changes from random orientation to {100} 〈120〉, eventually becoming a mixture of cube and Goss texture. The alloys treated at 1 and 2 T showed magnetic anisotropic behavior, while the alloy treated at 0 T showed magnetic isotropic behavior. The change in magnetic property comes from the evolution of α-Fe crystal orientation. Furthermore, a method for controlling the crystallization process and crystallographic orientation by adjusting the magnetic field intensity was proposed.

Keywords

Fe–6.5 Si–0.05 B alloymicrostructuretexturehigh magnetic fieldmagnetic property
Type
Article
Information
Journal of Materials Research , Volume 34 , Issue 24 , 30 December 2019 , pp. 4076 - 4084
Copyright
Copyright © Materials Research Society 2019 

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References

Honma, H., Ushigami, Y., and Suga, Y.: Magnetic properties of (110)[001] grain oriented 6.5% silicon steel. J. Appl. Phys. 70, 6259 (1991).CrossRefGoogle Scholar
Takada, Y., Abe, M., Masuda, S., and Inagaki, J.: Commercial scale production of Fe–6.5 wt% Si sheet and its magnetic properties. J. Appl. Phys. 64, 5367 (1988).CrossRefGoogle Scholar
Ouyang, G.Y., Chen, X., Liang, Y.F., Macziewski, C., and Cui, J.: Review of Fe–6.5 wt% Si high silicon steel-A promising soft magnetic material for sub-kHz application. J. Magn. Magn. Mater. 481, 234 (2019).CrossRefGoogle Scholar
Haiji, H., Okada, K., Hiratani, T., Abe, M., and Ninomiya, M.: Magnetic properties and workability of 6.5% Si steel sheet. J. Magn. Magn. Mater. 160, 109 (1996).10.1016/0304-8853(96)00128-XCrossRefGoogle Scholar
Zhang, Z.W., Chen, G., Bei, H., Ye, F., Chen, G.L., and Liu, C.T.: Improvement of magnetic properties of an Fe–6.5 wt% Si alloy by directional recrystallization. Appl. Phys. Lett. 93, 1908 (2008).CrossRefGoogle Scholar
Fu, H.D., Zhang, Z.H., Jiang, Y.B., and Xie, J.X.: Improvement of magnetic properties of an Fe–6.5 wt% Si alloy by directional solidification. Mater. Lett. 65, 1416 (2011).CrossRefGoogle Scholar
Zhang, Z.W., Chen, G., Bei, H., Li, F., Ye, F., and Chen, G.L.: Directional recrystallization and microstructures of an Fe–6.5 wt% Si alloy. J. Mater. Res. 24, 2654 (2009).CrossRefGoogle Scholar
Cui, S.L., Ouyang, G.Y., Ma, T., Macziewski, C., Levitas, V.I., Zhou, L., Kramer, M.J., and Cui, J.: Thermodynamic and kinetic analysis of the melt spinning process of Fe–6.5 wt% Si alloy. J. Alloys Compd. 771, 643 (2019).CrossRefGoogle Scholar
Ros, T., Ruiz, D., Houbaert, Y., and Vandenberghe, R.E.: Study of ordering phenomena in high silicon electrical steel (up to 12.5 at.%) by Mossbauer spectroscopy. J. Magn. Magn. Mater. 242, 208 (2002).CrossRefGoogle Scholar
Zhang, B., Liang, Y.F., Wen, S.B., Wang, S., Shi, X.J., Ye, F., and Lin, J.P.: High-strength low-iron-loss silicon steels fabricated by cold rolling. J. Alloys Compd. 481, 234 (2019).Google Scholar
Liang, Y.F., Ge, J.W., Fang, X.S., Ye, F., and Lin, J.P.: Hot deformation behavior and softening mechanism of Fe–6.5 wt% Si alloy. Mat. Sci. Eng., A 570, 8 (2013).CrossRefGoogle Scholar
Ros, T., Houbaert, Y., and De, M.: Evolution of magnetic properties and microstructure of high-silicon steel during hot dipping and diffusion annealing. IEEE Trans. Magn. 38, 3201 (2002).Google Scholar
Li, R., Shen, Q., Zhang, L.M., and Zhang, T.: Magnetic properties of high silicon iron sheet fabricated by direct powder rolling. J. Magn. Magn. Mater. 281, 135 (2004).CrossRefGoogle Scholar
Bouchara, D., Fagot, M., Degauque, J., and Bras, J.: Ordering influence on magnetic properties of rapidly quenched Fe–6.5 wt% Si. J. Magn. Magn. Mater. 83, 377 (1990).CrossRefGoogle Scholar
Liu, Y., Wang, Q., Kazuhiko, I., Yuan, Y., Liu, T., and He, J.C.: Magnetic-field-dependent microstructure evolution and magnetic properties of Tb0.27Dy0.73Fe1.95 alloy during solidification. J. Magn. Magn. Mater. 357, 18 (2014).CrossRefGoogle Scholar
Zheng, T.X., F Zhou, B., Wang, J., Shuai, S.S., Zhong, Y.B., Ren, W.L., Ren, Z.M., Debray, F., and Beaugnon, E.: Compression properties enhancement of Al–Cu alloy solidified under a 29 T high static magnetic field. Mat. Sci. Eng., A 733, 170 (2018).CrossRefGoogle Scholar
Wang, J., He, Y.X., Li, J.S., Li, C., Kou, H.C., Zhang, P.X., and Beaugnon, E.: Nucleation of supercooled Co melts under a high magnetic field. Mater. Chem. Phys. 225, 133 (2019).CrossRefGoogle Scholar
Rango, P.D., Lees, M., Lejay, P., Sulpice, A., Tournier, R., Ingold, M., Germi, P., and Pernet, M.J.N.: Texturing of magnetic materials at high temperature by solidification in a magnetic field. Nature 349, 770 (1991).CrossRefGoogle Scholar
Gao, P.F., Liu, T., Dong, M., Yuan, Y., and Wang, Q.: Magnetic domain structure, crystal orientation, and magnetostriction of Tb0.27Dy0.73Fe1.95 solidified in various high magnetic fields. J. Magn. Magn. Mater. 401, 755 (2016).CrossRefGoogle Scholar
Zheng, T.X., Zhong, Y.B., Lei, Z.S., Ren, W.L., Ren, Z.M., Wang, H., Wang, Q.L., Debray, F., Beaugnon, E., and Fautrelle, Y.: Effects of high static magnetic field on crystal orientation and magnetic property of Bi–5 wt% Zn alloys. Mater. Lett. 140, 68 (2015).CrossRefGoogle Scholar
Liu, C.M., Zhong, Y.B., Shen, Z., Dong, L.C., Zheng, T.X., Ren, W.L., Lei, Z.S., and Ren, Z.M.: Effect of a transverse weak magnetic field on the texture evolution and magnetic property of Fe–1.0 wt% Si alloy during bulk solidification. Mater. Res. Express 6, 6 (2019).Google Scholar
Fu, H.D., Zhang, Z.H., Wu, X.S., and Xie, J.X.: Effects of boron on microstructure and mechanical properties of Fe–6.5 wt% Si alloy fabricated by directional solidification. Intermetallics 35, 67 (2013).CrossRefGoogle Scholar
Fu, H.D., Yang, Q., Zhang, Z.H., and Xie, J.X.: Effects of precipitated phase and order degree on bending properties of an Fe–6.5 wt% Si alloy with columnar grains. J. Mater. Res. 26, 1711 (2011).CrossRefGoogle Scholar
Fu, H.D., Zhang, Z.H., Yang, Q., and Xie, J.X.: Morphology of the boron-rich phase along columnar grain boundary and its effects on the compression crack of Fe–6.5Si–0.05B alloy. Mat. Sci. Eng., A 528, 1425 (2011).CrossRefGoogle Scholar
Kim, K.N., Pan, L.M., Lin, J.P., Wang, Y.L., Lin, Z., and Chen, G.L.: The effect of boron content on the processing for Fe–6.5 wt% Si electrical steel sheets. J. Magn. Magn. Mater. 277, 331 (2004).CrossRefGoogle Scholar
Utech, H.P. and Flemings, M.C.: Elimination of solute banding in indium antimonide crystals by growth in a magnetic field. J. Appl. Phys. 37, 2021 (1966).CrossRefGoogle Scholar
Asai, S., Sassa, K.S., and Tahashi, M.: Crystal orientation of non-magnetic materials by imposition of a high magnetic field. Sci. Technol. Adv. Mater. 4, 455 (2003).CrossRefGoogle Scholar
Wang, C.J., Wang, Q., Wang, Z.Y., Li, H.T., Nakajima, K.J., and He, J.C.: Phase alignment and crystal orientation of Al3Ni in Al–Ni alloy by imposition of a uniform high magnetic field. J. Cryst. Growth 310, 1256 (2008).CrossRefGoogle Scholar
Mathiak, G. and Frohberg, G.: Interdiffusion and convection in high magnetic fields. Cryst. Res. Technol. 34, 181 (1999).3.0.CO;2-1>CrossRefGoogle Scholar
Li, X., Ren, Z.M., Fautrelle, Y., Zhang, Y.D., and Esling, C.: Morphological instabilities and alignment of lamellar eutectics during directional solidification under a strong magnetic field. Acta Mater. 58, 1403 (2010).CrossRefGoogle Scholar
Sandoval Robles, J.A., Salas Zamarripa, A., Guerrero Mata, M.P., and Cabrera, J.: Texture evolution of experimental silicon steel grades. Part I: Hot rolling. J. Magn. Magn. Mater. 429, 367 (2017).CrossRefGoogle Scholar
Sun, Z.H.I., Guo, M., Vleugels, J., Van, O., and Blanpain, B.: Strong static magnetic field processing of metallic materials: A review. Curr. Opin. Solid State Mater. Sci. 16, 254 (2012).CrossRefGoogle Scholar
Mikelson, A.E. and Karklin, Y.K.: Control of crystallization processes by means of magnetic fields. J. Cryst. Growth 52, 524 (1981).CrossRefGoogle Scholar
Stojakovic, D., Doherty, R.D., Kalidindi, S.R., and Landgraf, F.J.G.: Thermomechanical processing for recovery of desired 〈001〉 fiber texture in electric motor steels. Metall. Mater. Trans. A 39, 1738 (2008).CrossRefGoogle Scholar
Umakoshi, Y. and Kronmuller, H.: On magnetic domain patterns and dislocation structures in iron crystals deformed at 196 and 77 K. Phys. Status Solidi 68, 159 (1981).CrossRefGoogle Scholar
Hayashi, S. and Echigoya, J.: Microscopic behaviors of magnetic domain walls in Co–Fe alloy and Co–Gd eutectic. Phys. Status Solidi 184, 211 (2001).3.0.CO;2-L>CrossRefGoogle Scholar