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Indentation size effect in aqueous electrophoretic deposition zirconia dental ceramic

Published online by Cambridge University Press:  10 January 2019

Lei Wang ,
Isaac Asempah ,
Xu Li ,
Sheng-Qi Zang ,
Yan-Fei Zhou ,
Jie Ding  and
Lei Jin
Lei Wang*
Affiliation:
Stomatology Department, Nanjing General Hospital, Medical School, Nanjing University, Nanjing 210002, People’s Republic of China; and National Demonstration Center for Experimental Materials Science and Engineering Education, Jiangsu University of Science and Technology, Zhenjiang 212003, People’s Republic of China
Isaac Asempah
Affiliation:
National Demonstration Center for Experimental Materials Science and Engineering Education, Jiangsu University of Science and Technology, Zhenjiang 212003, People’s Republic of China
Xu Li
Affiliation:
National Demonstration Center for Experimental Materials Science and Engineering Education, Jiangsu University of Science and Technology, Zhenjiang 212003, People’s Republic of China
Sheng-Qi Zang
Affiliation:
Stomatology Department, Nanjing General Hospital, Medical School, Nanjing University, Nanjing 210002, People’s Republic of China
Yan-Fei Zhou
Affiliation:
National Demonstration Center for Experimental Materials Science and Engineering Education, Jiangsu University of Science and Technology, Zhenjiang 212003, People’s Republic of China
Jie Ding
Affiliation:
National Demonstration Center for Experimental Materials Science and Engineering Education, Jiangsu University of Science and Technology, Zhenjiang 212003, People’s Republic of China
Lei Jin*
Affiliation:
Stomatology Department, Nanjing General Hospital, Medical School, Nanjing University, Nanjing 210002, People’s Republic of China
*
a)Address all correspondence to these authors. e-mail: [email protected]
b)e-mail: [email protected]
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Abstract

Highly dense zirconia dental ceramic coatings were fabricated by aqueous electrophoretic deposition (EPD) and subsequently sintered between 1250 and 1450 °C. Microstructural examination revealed that aqueous EPDZrO2 coatings possessed a tetragonal phase structure and the grain size increased with increasing sintering temperature. Nanoindentation study proved that the aqueous EPDZrO2 coating also had excellent mechanical properties. The effect of different applied loads on hardness and elastic modulus of the 1350 °C-sintered sample at room temperature was investigated by the method of progressive multicycle measurement nanoindentation. The simulative experiment proved that hardness of aqueous EPDZrO2 exhibited reverse indentation size effect (ISE) behavior and then displayed the normal ISE response. The analysis indicates that the reverse ISE is attributed to the relaxation of surface stresses resulting from indentation cracks at small loads and normal ISE is caused by geometrically necessary dislocations. The tetragonal–monoclinic stress-induced phase transformation during nanoindentation is the primary cause of dental zirconia failures.

Keywords

nanoindentationelectrodepositionceramic
Type
Article
Information
Journal of Materials Research , Volume 34 , Issue 4 , 28 February 2019 , pp. 555 - 562
Copyright
Copyright © Materials Research Society 2019 

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