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Formation process of calcium vanadate nanorods and their electrochemical sensing properties

Published online by Cambridge University Press:  31 July 2012

Lizhai Pei ,
Yinqiang Pei ,
Yikang Xie ,
Chuangang Fan ,
Diankai Li  and
Qianfeng Zhang
Lizhai Pei*
Affiliation:
Key Lab of Materials Science and Processing of Anhui Province, Institute of Molecular Engineering and Applied Chemistry, School of Materials Science and Engineering, Anhui University of Technology, Ma’anshan, Anhui 243002, People’s Republic of China
Yinqiang Pei
Affiliation:
Key Lab of Materials Science and Processing of Anhui Province, Institute of Molecular Engineering and Applied Chemistry, School of Materials Science and Engineering, Anhui University of Technology, Ma’anshan, Anhui 243002, People’s Republic of China
Yikang Xie
Affiliation:
Key Lab of Materials Science and Processing of Anhui Province, Institute of Molecular Engineering and Applied Chemistry, School of Materials Science and Engineering, Anhui University of Technology, Ma’anshan, Anhui 243002, People’s Republic of China
Chuangang Fan
Affiliation:
Key Lab of Materials Science and Processing of Anhui Province, Institute of Molecular Engineering and Applied Chemistry, School of Materials Science and Engineering, Anhui University of Technology, Ma’anshan, Anhui 243002, People’s Republic of China
Diankai Li
Affiliation:
Key Lab of Materials Science and Processing of Anhui Province, Institute of Molecular Engineering and Applied Chemistry, School of Materials Science and Engineering, Anhui University of Technology, Ma’anshan, Anhui 243002, People’s Republic of China
Qianfeng Zhang
Affiliation:
Key Lab of Materials Science and Processing of Anhui Province, Institute of Molecular Engineering and Applied Chemistry, School of Materials Science and Engineering, Anhui University of Technology, Ma’anshan, Anhui 243002, People’s Republic of China
*
a)Address all correspondence to this author. e-mail: [email protected], [email protected]
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Abstract

Calcium vanadate nanorods with Ca10V6O25 phase have been synthesized by a hydrothermal process without any surfactants. Hydrothermal temperature, reaction time and calcium (Ca) raw materials play important roles in the formation and size of the calcium vanadate nanorods. The nucleation and crystal growth combined with crystal splitting process have been proposed to explain the formation and growth of calcium vanadate nanorods. The calcium vanadate nanorods are used as glassy carbon electrode-modified materials to analyze the electrochemical behaviors of tartaric acid. The calcium vanadate nanorod-modified glassy carbon electrode exhibits good performance for the electrochemical detection of tartaric acid with a detection limit of 2.4 μM and linear range of 0.005–2 mM. The analytical performance and straightforward fabrication method make the calcium vanadate nanorods promising for the development of electrochemical sensors for tartaric acid.

Type
Articles
Information
Journal of Materials Research , Volume 27 , Issue 18 , 28 September 2012 , pp. 2391 - 2400
Copyright
Copyright © Materials Research Society 2012

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