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Electrical technique for monitoring crack growth in thin-film fracture mechanics specimens

Published online by Cambridge University Press:  01 November 2004

Eric P. Guyer
Affiliation:
Department of Materials Science and Engineering, Stanford University, Stanford, California 94305
Reinhold H. Dauskardt*
Affiliation:
Department of Materials Science and Engineering, Stanford University, Stanford, California 94305
*
a) Address all correspondence to this author. e-mail: [email protected]
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Abstract

An accurate and reliable electrical technique for continuous monitoring of crack growth in fracture specimens containing technologically relevant thin-film device structures has been developed. Both adhesive and cohesive crack growth measurements are reported using a SiO2 passivation layer and a conducting titanium film deposited on the side face of fracture specimens. Crack velocity measurements approaching 10−12 m/s were achieved, representing nearly an order of magnitude improvement over commonly used compliance-based techniques. The technique may be particularly useful for elucidating near threshold crack velocity behavior, which is important for thin-film reliability.

Type
Rapid Communications
Copyright
Copyright © Materials Research Society 2004

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References

REFERENCES

1.Guyer, E.P., Dauskardt, R.H.: Fracture of nanoporous thin-film glasses. Nat. Mater. 3, 53 (2004).CrossRefGoogle ScholarPubMed
2.Snodgrass, J.M., Pantelidis, D., Jenkins, M.L., Bravman, J.C., Dauskardt, R.H.: Subcritical debonding of polymer/silica interfaces under monotonic and cyclic loading. Acta Mater. 50, 2395 (2002).CrossRefGoogle Scholar
3.Kook, S.Y., Dauskardt, R.H.: Moisture-assisted subcritical debonding of a polymer/metal interface. J. Appl. Phys. 91, 1293 (2002).CrossRefGoogle Scholar
4.Dauskardt, R.H., Lane, M., Ma, Q., Krishna, N.: Adhesion and debonding of multi-layer thin film structures. Engineering Fracture Mechanics 61, 141 (1998).CrossRefGoogle Scholar
5.Cook, R.F., Liniger, E.G.: Kinetics of indentation cracking in glass. J. Am. Ceram. Soc. 76, 1096 (1993).CrossRefGoogle Scholar
6.Cook, R., Liniger, E.: Stress-corrosion cracking of low-dielectric constant spin-on-glass thin films. J. Electrochem. Soc. 146, 4439 (1999).CrossRefGoogle Scholar
7.Lin, Y., Vlassak, J., Tsui, T., McKerrow, A.: Environmental Effects on Subcritical Delamination of Dielectric and Metal Films from Organosilicate Glass (OSG) Thin Films. (Materials Research Society, Warrendale, PA, 2003).Google Scholar
8.Muhlstein, C.L., Stach, E.A., Ritchie, R.O.: Mechanism of fatigue in micron-scale films of polycrystalline silicon for microelectromechanical systems. Appl. Phys. Lett. 80, 1532 (2002).CrossRefGoogle Scholar
9.Lane, M.: Interface fracture. Annu. Rev. Mater. Res. 33, 29 (2003).CrossRefGoogle Scholar
10.Lane, M., Ware, R., Voss, S., Ma, Q., Fujimoto, H., Dauskardt, R.H.: Materials Reliability in Microelectronics VII Symposium (Materials Research Society, San Francisco, CA, 1997).Google Scholar
11.Lane, M.W., Snodgrass, J.M., Dauskardt, R.H.: Environmental effects on interfacial adhesion. Microelectron Reliab. 41, 1615 (2001).CrossRefGoogle Scholar
12.Kanninen, M.F.: Augmented double cantilever beam model for studying crack-propagation and arrest. International Journal of Fracture 9, 83 (1973).CrossRefGoogle Scholar
13.Mroz, J., Dauskardt, R.H., Schleinkofer, U.: New adhesion measurement technique for coated cutting tool materials. Int. J. Refract. Met. Hard Mater. 16, 395 (1998).CrossRefGoogle Scholar
14.Aronson, G.H., Ritchie, R.O.: Optimization of the electrical potential technique for crack growth monitoring in compact test pieces using finite element analysis. J. Test. Eval. 7, 208 (1979).CrossRefGoogle Scholar
15.Hartman, G., Johnson, D.: D-C electric-potential method applied to thermal/mechanical fatigue crack growth. Experimental Mechanics 27, 106 (1987).CrossRefGoogle Scholar
16.Dauskardt, R.H., Yu, W., Ritchie, R.O.: Fatigue-crack propagation in transformation-toughened zirconia ceramic. J Am. Ceram. Soc. 70, C248 (1987).CrossRefGoogle Scholar
17.Dill, S.J., Bennison, S.J., Dauskardt, R.H.: Subcritical crack-growth behavior of borosilicate glass under cyclic loads: Evidence of a mechanical fatigue effect. J Am. Ceram. Soc. 80, 773 (1997).CrossRefGoogle Scholar
18.Fitzgerald, A.M., Dauskardt, R.H., Kenny, T.W.: Fracture toughness and crack growth phenomena of plasma-etched single crystal silicon. Sens. Actuators A Phys. 83, 194 (2000).CrossRefGoogle Scholar
19.Kanninen, M.F.: An augmented double cantilever beam model for studying crack propagation and arrest. International Journal of Fracture 9, 83 (1973).CrossRefGoogle Scholar
20.Wiederhorn, S.M.: Influence of water vapor on crack propagation in soda-lime glass. J Am. Ceram. Soc. 50, 407 (1967).CrossRefGoogle Scholar
21.Lawn, B.R.: Fracture of Brittle Solids (Cambridge University Press, Cambridge, U.K., 1993).Google Scholar
22.Lane, M., Dauskardt, R.H., Krishna, N., Hashim, I.: Adhesion and reliability of copper interconnects with Ta and TaN barrier layers. J. Mater. Res. 15, 203 (2000).CrossRefGoogle Scholar