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Effects of pre-treatments on precipitate microstructures and creep-rupture behavior of an Al–Zn–Mg–Cu alloy

Published online by Cambridge University Press:  15 April 2016

Y.C. Lin*
Affiliation:
School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China; Light Alloy Research Institute of Central South University, Changsha 410083, China; and State Key Laboratory of High Performance Complex Manufacturing, Changsha 410083, China
Zong-Wei Wang
Affiliation:
Light Alloy Research Institute of Central South University, Changsha 410083, China
Dao-Guang He
Affiliation:
Light Alloy Research Institute of Central South University, Changsha 410083, China
Ying Zhou
Affiliation:
School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China
Ming-Song Chen
Affiliation:
School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China; and State Key Laboratory of High Performance Complex Manufacturing, Changsha 410083, China
Ming-Hui Huang
Affiliation:
School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China; Light Alloy Research Institute of Central South University, Changsha 410083, China; and State Key Laboratory of High Performance Complex Manufacturing, Changsha 410083, China
Jin-Long Zhang
Affiliation:
School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China; and State Key Laboratory of High Performance Complex Manufacturing, Changsha 410083, China
*
a) Address all correspondence to this author. e-mail: [email protected], [email protected]
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Abstract

The effects of pre-treatments on the precipitate microstructures of an Al–Zn–Mg–Cu alloy are investigated. Meanwhile, the creep-rupture behavior of the under-aged and peak-aged alloys are comparatively analyzed. Additionally, the effects of pre-treatment on the fracture mechanisms are discussed. It is found that the precipitate microstructures are sensitive to pre-treatments. The intragranular precipitates of the peak-aged alloy are larger than those of the under-aged. The precipitate free zone of the peak-aged alloy is wider than that of the under-aged. Some large intergranular precipitates appear on the grain boundaries of the under-aged alloy, and induce the nucleation of microvoids. Eventually, the creep fracture of the under-aged alloy is accelerated. Therefore, the differences in microstructures lead to the shorter creep-rupture life of the under-aged alloy, compared to the peak-aged alloy.

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Articles
Copyright
Copyright © Materials Research Society 2016 

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References

REFERENCES

Lin, Y.C., Li, L.T., Xia, Y.C., and Jiang, Y.Q.: Hot deformation and processing map of a typical Al–Zn–Mg–Cu alloy. J. Alloys Compd., 550, 438 (2013).CrossRefGoogle Scholar
Shaeri, M.H., Salehi, M.T., Seyyedein, S.H., Abutalebi, M.R., and Park, J.K.: Microstructure and mechanical properties of Al-7075 alloy processed by equal channel angular pressing combined with aging treatment. Mater. Des., 57, 250 (2014).Google Scholar
Shi, C.J., Lai, J., and Chen, X.G.: Microstructural evolution and dynamic softening mechanisms of Al–Zn–Mg–Cu alloy during hot compressive deformation. Materials, 7, 244 (2014).Google Scholar
Rokni, M.R., Zarei-Hanzaki, A., Widener, C.A., and Changizian, P.: The strain-compensated constitutive equation for high temperature flow behavior of an Al–Zn–Mg–Cu alloy. J. Mater. Eng. Perform. 23, 4002 (2014).Google Scholar
Lin, Y.C. and Chen, X.M.: A critical review of experimental results and constitutive descriptions for metals and alloys in hot working. Mater. Des. 32, 1733 (2011).Google Scholar
Elkhodary, K., Lee, W., Sun, L.P., Brenner, D.W., and Zikry, M.A.: Deformation mechanisms of an Ω precipitate in a high-strength aluminum alloy subjected to high strain rates. J. Mater. Res. 26, 487 (2011).Google Scholar
Naser, T.S.B. and Krallics, G.: Mechanical behavior of multiple-forged Al 7075 aluminum alloy. Acta Polytech. Hung. 11, 103 (2014).Google Scholar
Haghdadi, N., Zarei-Hanzaki, A., Abedi, H.R., and Sabokpa, O.: The effect of thermomechanical parameters on the eutectic silicon characteristics in a non-modified cast A356 aluminum alloy. Mater. Sci. Eng., A. 549, 93 (2012).Google Scholar
Huo, W.T., Hou, L.G., Cui, H., Zhuang, L.Z., and Zhang, J.S.: Fine-grained AA 7075 processed by different thermo-mechanical processing. Mater. Sci. Eng., A. 618, 244 (2014).Google Scholar
Shaeri, M.H., Salehi, M.T., Seyyedein, S.H., Abutalebi, M.R., and Park, J.K.: Characterization of microstructure and deformation texture during equal channel Angular pressing of Al–Zn–Mg–Cu alloy. J. Alloys Compd. 576, 350 (2013).Google Scholar
Shaterani, P., Zarei-Hanzaki, A., Fatemi-Varzaneh, S.M., and Hassas-Irani, S.B.: The second phase particles and mechanical properties of 2124 aluminum alloy processed by accumulative back extrusion. Mater. Des. 58, 535 (2014).Google Scholar
Park, J.K. and Ardell, A.J.: Microchemical analysis of precipitate free zones in 7075-A1 in the T6, T7 and RRA tempers. Acta Mater. 39, 591 (1991).Google Scholar
Sankaran, K.K., Perez, R., and Jata, K.V.: Effects of pitting corrosion on the fatigue behavior of aluminum alloy 7075-T6: Modeling and experimental studies. Mater. Sci. Eng., A. 297, 223 (2001).CrossRefGoogle Scholar
Shi, Y.J., Pan, Q.L., Li, M.J., Huang, X., and Li, B.: Effect of Sc and Zr additions on corrosion behaviour of Al–Zn–Mg–Cu alloys. J. Alloys Compd. 612, 42 (2014).Google Scholar
El-Amoush, A.S.: Investigation of corrosion behaviour of hydrogenated 7075-T6 aluminum alloy. J. Alloys Compd. 443, 171 (2007).CrossRefGoogle Scholar
El-Amoush, A.S.: Intergranular corrosion behavior of the 7075-T6 aluminum alloy under different annealing conditions. Mater. Chem. Phys. 126, 607 (2011).Google Scholar
Marlaud, T., Deschamps, A., Bley, F., Lefebvre, W., and Baroux, B.: Evolution of precipitate microstructures during the retrogression and re-ageing heat treatment of an Al–Zn–Mg–Cu alloy. Acta Mater. 58, 4814, (2010).Google Scholar
Yang, W.C., Ji, S.X., Zhang, Q., and Wang, M.P.: Investigation of mechanical and corrosion properties of an Al-Zn-Mg-Cu alloy under various ageing conditions and interface analysis of η’ precipitate. Mater. Des. 85, 752 (2015).Google Scholar
Li, J.F., Birbilis, N., Li, C.X., Jia, Z.Q., Cai, B., and Zheng, Z.Q.: Influence of retrogression temperature and time on the mechanical properties and exfoliation corrosion behavior of aluminium alloy AA7150. Mater. Charact. 60, 1334 (2009).Google Scholar
Lin, Y.C., Zhang, J.L., Liu, G., and Liang, Y.J.: Effects of pre-treatments on aging precipitates and corrosion resistance of a creep-aged Al–Zn–Mg–Cu alloy. Mater. Des. 83, 866 (2015).Google Scholar
Lin, Y.C., Liu, G., Chen, M.S., Huang, Y.C., Chen, Z.G., Ma, X., Jiang, Y.Q., and Li, J.: Corrosion resistance of a two-stage stress-aged Al-Cu-Mg alloy: Effects of stress-aging temperature. J. Alloys Compd. 657, 855 (2016).Google Scholar
Lin, Y.C., Jiang, Y.Q., Chen, X.M., Wen, D.X., and Zhou, H.M.: Effect of creep-aging on precipitates of 7075 aluminum alloy. Mater. Sci. Eng., A. 588, 347 (2013).Google Scholar
Li, L.T., Lin, Y.C., Zhou, H.M., Xia, Y.C., and Jiang, Y.Q.: Modeling the high-temperature creep behaviors of 7075 and 2124 aluminum alloys by continuum damage mechanics model. Comput. Mater. Sci. 73, 72 (2013).Google Scholar
Maximov, J.T., Duncheva, G.V., Anchev, A.P., and Ichkova, M.D.: Modeling of strain hardening and creep behaviour of 2024T3 aluminium alloy at room and high temperatures. Comput. Mater. Sci. 83, 381 (2014).CrossRefGoogle Scholar
Maximov, J.T., Duncheva, G.V., and Anchev, A.P.: An approach to modeling time-dependent creep and residual stress relaxation around cold worked holes in aluminium alloys at room temperature. Eng. Failure Anal. 45, 1 (2014).Google Scholar
Jiang, Y.Q., Lin, Y.C., Phaniraj, C., Xia, Y.C., and Zhou, H.M.: Creep and creep–rupture behavior of 2124-T851 aluminum alloy. High Temp. Mater. Processes 32, 533 (2013).Google Scholar
Lin, Y.C., Xia, Y.C., Ma, X.S., Jiang, Y.Q., and Chen, M.S.: High-temperature creep behavior of Al-Cu-Mg alloy. Mater. Sci. Eng., A. 550, 125 (2012).Google Scholar
Mahathaninwong, N., Zhou, Y., Babcock, S.E., Plookphol, T., Wannasin, J., and Wisutmethangoon, S.: Creep rupture behavior of semi-solid cast 7075-T6 Al alloy. Mater. Sci. Eng., A. 556, 107 (2012).Google Scholar
Yousefiani, A., Mohamed, F.A., and Earthman, J.C.: Creep rupture mechanisms in annealed and overheated 7075 Al under multiaxial stress states. Metall. Mater. Trans. 31, 2807 (2000).Google Scholar
Srivastava, V., Williams, J.P., McNee, K.R., Greenwood, G.W., and Jones, H.: Low stress creep behaviour of 7075 high strength aluminium alloy. Mater. Sci. Eng., A. 382, 50 (2004).CrossRefGoogle Scholar
Leacock, A.G., Howe, C., Brown, D., Lademob, O.G., and Deering, A.: Evolution of mechanical properties in a 7075 Al-alloy subject to natural ageing. Mater. Des. 49, 160 (2013).CrossRefGoogle Scholar
Buha, J., Lumley, R.N., and Crosky, A.G.: Secondary ageing in an aluminium alloy 7050. Mater. Sci. Eng., A. 492, 1 (2008).CrossRefGoogle Scholar
Florando, J.N., Margraf, J.D., Reus, J.F., Anderson, A.T., McCallen, R.C., LeBlanc, M.M., Stanley, J.R., Rubenchik, A.M., Wu, S.S., and Lowdermilk, W.H.: Modeling the effect of laser heating on the strength and failure of 7075-T6 aluminum. Mater. Sci. Eng., A. 640, 402 (2015).Google Scholar
Liu, Y., Jiang, D., Li, B., Yang, W.S., and Hu, J.: Effect of cooling aging on microstructure and mechanical properties of an Al–Zn–Mg–Cu alloy. Mater. Des. 57, 79 (2014).Google Scholar
Danh, N.C., Rajan, K., and Wallace, W.: A TEM study of microstructural changes during retrogression and reaging in 7075 aluminum. Metall. Mater. Trans. 14, 1843 (1983).CrossRefGoogle Scholar
Li, J.F., Peng, Z.W., Li, C.X., Jia, Z.Q., Chen, W.J., and Zheng, Z.Q.: Mechanical properties, corrosion behaviors and microstructures of 7075 aluminium alloy with various aging treatments. Trans. Nonferrous Met. Soc. China 18, 755 (2008).CrossRefGoogle Scholar
Park, J.K. and Ardell, A.J.: Precipitate microstructure of peak-aged 7075 Al. Scr. Mater. 22, 1115 (1988).Google Scholar
Du, Z.W., Sun, Z.M., Shao, B.L., Zhou, T.T., and Chen, C.Q.: Quantitative evaluation of precipitates in an Al–Zn–Mg–Cu alloy after isothermal ageing. Mater. Charact. 56, 121 (2006).Google Scholar
Li, M.H., Yang, Y.Q., Feng, Z.Q., Huang, B., Luo, X., Lou, J.H., and Ru, J.G.: Precipitation sequence of η phase along low-angle grain boundaries in Al-Zn-Mg-Cu alloy during artificial aging. Trans. Nonferrous Met. Soc. China 24, 2061 (2014).CrossRefGoogle Scholar
Xu, X.F., Zhao, Y.G., Ma, B.D., and Zhang, M.: Electropulsing induced evolution of grain-boundary precipitates without loss of strength in the 7075 Al alloy. Mater. Charact. 105, 90 (2015).Google Scholar
Lejcek, P.: Grain boundary segregation in metals, 1st ed. (Springer, Berlin, Germany, 2010); pp. 173201.CrossRefGoogle Scholar
Faulkner, R.G.: Segregation to boundaries and interfaces in solids. Int. Mater. Rev. 41, 198 ( 1996).Google Scholar
Panseri, C., Gatto, F., and Federighi, T.: Interaction between solute magnesium atoms and vacancies in aluminium. Acta Metall. 6, 198 (1958).Google Scholar
Panseri, C. and Federighi, T.: Evidence for the interaction between Mg atoms and vacancies in Al–Zn 10%–Mg 0.1% alloy. Acta Metall. 11, 575 (1963).Google Scholar
Xu, T.D., Wang, K., and Song, S.H.: Theoretical progress in non-equilibrium grain-boundary segregation (I): Thermally induced non-equilibrium grain-boundary segregation and intergranular embrittlement. Sci. China, Ser. E: Technol. Sci. 52, 893(2009).Google Scholar
Bakker, H., Bonzel, H.P., Bruff, C.M., Dayananda, M.A., Gust, W., Horváth, J., Kaur, I., Kidson, G.V., LeClaire, A.D., Mehrer, H., Murch, G.E., Neumann, G., Stolica, N., and Stolwijk, N.A.: Diffusion in solid metals and alloys, 1st ed. Vol. 26, (Springer, Berlin, Germany, 1990); pp. 710.Google Scholar
Marlaud, T., Deschamps, A., Bley, F., Lefebvre, W., and Baroux, B.: Influence of alloy composition and heat treatment on precipitate composition in Al–Zn–Mg–Cu alloys. Acta Mater. 58, 248 (2010).CrossRefGoogle Scholar
Ratke, L. and Voorhees, P.W.: Growth and coarsening: Ostwald ripening in material processing, 1st ed. (Springer, Berlin, Germany, 2013); pp. 150193.Google Scholar
Oriani, R.A.: Ostwald ripening of precipitates in solid matrices. Acta Mater. 12, 1399 (1964).Google Scholar
Dorward, R.C.: Precipitate coarsening during overaging of Al–Zn–Mg–Cu alloy. Mater. Sci. Technol. 15, 1133 (1999).Google Scholar
Fribourg, G., Bréchet, Y., Chemin, J.L., and Deschamps, A.: Evolution of precipitate microstructure during creep of an AA7449 T7651 aluminum alloy. Metall. Mater. Trans. 42, 3934 (2011).CrossRefGoogle Scholar
Kahlweit, M.: Ostwald ripening of precipitates. Adv. Colloid Interface Sci. 5, 35 (1975).CrossRefGoogle Scholar
Voorhees, P.W.: The theory of Ostwald ripening. J. Stat. Phys. 38, 231 (1985).CrossRefGoogle Scholar
Zhou, M., Lin, Y.C., Deng, J., and Jiang, Y.Q.: Hot tensile deformation behaviors and constitutive model of an Al–Zn–Mg–Cu alloy. Mater. Des. 59, 141 (2014).CrossRefGoogle Scholar
Kassner, M.E. and Hayes, T.A.: Creep cavitation in metals. Int. J. Plast. 19, 1715 (2003).Google Scholar