Hostname: page-component-586b7cd67f-l7hp2 Total loading time: 0 Render date: 2024-11-24T11:15:29.477Z Has data issue: false hasContentIssue false

Effects of dynamic indentation on the mechanical response of materials

Published online by Cambridge University Press:  31 January 2011

M.J. Cordill*
Affiliation:
Erich Schmid Institute for Materials Science, Austrian Academy of Sciences, University of Leoben, Leoben A-8700, Austria; and Department of Chemical Engineering & Materials Science, University of Minnesota, Minneapolis, Minnesota 55455
N.R. Moody
Affiliation:
Sandia National Laboratories, Livermore, California 94551-0969
W.W. Gerberich
Affiliation:
Department of Chemical Engineering & Materials Science, University of Minnesota, Minneapolis, Minnesota 55455
*
a)Address all correspondence to this author. e-mail: [email protected]
Get access

Abstract

Dynamic indentation techniques are often used to determine mechanical properties as a function of depth by continuously measuring the stiffness of a material. The dynamics are used by superimposing an oscillation on top of the monotonic loading. Of interest was how the oscillation affects the measured mechanical properties when compared to a quasi-static indent run at the same loading conditions as a dynamic. Single crystals of nickel and NaCl as well as a polycrystalline nickel sample and amorphous fused quartz and polycarbonate have all been studied. With respect to dynamic oscillations, the result is a decrease of the load at the same displacement and thus lower measured hardness values of the ductile crystalline materials. It has also been found that the first 100 nm of displacement are the most affected by the oscillating tip, an important length scale for testing thin films, nanopillars, and nanoparticles.

Type
Articles
Copyright
Copyright © Materials Research Society 2008

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1Oliver, W.C.Pharr, G.M.: An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7, 1564 1992CrossRefGoogle Scholar
2Fischer-Cripps, A.C.: Multiple-frequency dynamic nanoindentation testing. J. Mater. Res. 19, 2981 2004CrossRefGoogle Scholar
3Jungk, J.M., Mook, W.M., Cordill, M.J., Chambers, M.D., Gerberich, W.W., Bahr, D.F., Moody, N.R.Hoehn, J.W.: Length-scale-based hardening model for ultra-small volumes. J. Mater. Res. 19, 2812 2004CrossRefGoogle Scholar
4Cheng, Y.T., Ni, W.Cheng, C.M.: Nonlinear analysis of oscillatory indentation in elastic and viscoelastic solids. Phys. Rev. Lett. 97, 075506-1 2006CrossRefGoogle ScholarPubMed
5VanLandingham, M.R., Chang, N.K., Drzal, P.L., White, C.C.Chang, S.H.: Viscoelastic characterization of polymers using instrumented indentation. I. Quasi-static testing. J. Polym. Sci., Part B: Polym. Phys. 43, 1794 2005CrossRefGoogle Scholar
6White, C.C., VanLandingham, M.R., Drzal, P.L., Chang, N.K.Chang, S.H.: Viscoeleastic characterization of polymers using instrumented indentation. II. Dynamic testing. J. Polym. Sci., Part B: Polym. Phys. 43, 1812 2005CrossRefGoogle Scholar
7Mencik, J., Rauchs, G., Bardon, J.Riche, A.: Determination of elastic modulus and hardness of viscoelastic-plastic materials by instrumented indentation under harmonic load. J. Mater. Res. 20, 2660 2005CrossRefGoogle Scholar
8Ebenstein, D.M.Wahl, K.J.: A comparison of JKR-based methods to analyze quasi-static and dynamic indentation force curves. J. Colloid Interface Sci. 298, 652 2006CrossRefGoogle ScholarPubMed
9Fischer-Cripps, A.C.: Nanoindentation Springer Verlag New York 2004CrossRefGoogle Scholar
10Page, T.F., Pharr, G.M., Hay, J.C., Oliver, W.C., Lucas, B.N., Herbert, E.Riester, L.: Nanoindentation characterisation of coated systems: P/S2. A new approach using the continuous stiffness technique in Fundamentals of Nanoindentation and Nanotribology, edited by N.R. Moody, W.W. Gerberich, N. Burnham, and S.P. Baker (Mater. Res. Soc. Symp. Proc. 522, Warrendale, PA, 1998), p. 53–64CrossRefGoogle Scholar
11Cordill, M.J., Moody, N.R.Gerberich, W.W.: The role of dislocation walls for nanoindentation to shallow depths. Int. J. Plasticity 2008 in pressGoogle Scholar
12Chen, J.Bull, S.J.: On the relationship between plastic zone radius and maximum depth during nanoindentation. Surf. Coat. Technol. 201, 4289 2006CrossRefGoogle Scholar
13Navamathavan, R., Kim, K.K., Hwang, D.K., Park, S.J., Hahn, J.H., Lee, T.G.Kim, G.S.: A nanoindentation study of the mechanical properties of ZnO thin films on (0001) sapphire. Appl. Surf. Sci. 253, 464 2006CrossRefGoogle Scholar
14Chudoba, T., Schwaller, P., Rabe, R., Breguet, J.M.Michler, J.: Comparison of nanoindentation results obtained with berkovich and cube-corner indenters. Philos. Mag. 86, 5265 2006CrossRefGoogle Scholar
15Mirshams, R.A.Pothapragada, R.M.: Correlation of nanoindentation measurements of nickel made using geometrically different indenter tips. Acta Mater. 54, 1123 2006CrossRefGoogle Scholar
16Oliver, W.C.Pharr, G.M.: Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology. J. Mater. Res. 19, 3 2004CrossRefGoogle Scholar
17Johnson, K.L.: Contact Mechanics Cambridge University Press Cambridge, UK 1985CrossRefGoogle Scholar