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Characterization of yttrium aluminate garnet precursors synthesized via precipitation using ammonium bicarbonate as the precipitant

Published online by Cambridge University Press:  31 January 2011

Ji-Guang Li ,
Takayasu Ikegami ,
Jong-Heun Lee  and
Toshiyuki Mori
Ji-Guang Li*
Affiliation:
National Institute for Research in Inorganic Materials, Namiki 1–1, Tsukuba, Ibaraki 305–0044, Japan
Takayasu Ikegami
Affiliation:
National Institute for Research in Inorganic Materials, Namiki 1–1, Tsukuba, Ibaraki 305–0044, Japan
Jong-Heun Lee
Affiliation:
National Institute for Research in Inorganic Materials, Namiki 1–1, Tsukuba, Ibaraki 305–0044, Japan
Toshiyuki Mori
Affiliation:
National Institute for Research in Inorganic Materials, Namiki 1–1, Tsukuba, Ibaraki 305–0044, Japan
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

Stoichiometric yttrium aluminate garnet (Y3Al5O12) precursors with a wide range of chemical compositions were precipitated by dripping a mixed solution of ammonium aluminum sulfate and yttrium nitrate into ammonium bicarbonate solutions. The resultant precursors were characterized by chemical analysis, infrared spectroscopy, differential thermal analysis/thermogravimetry, x-ray diffractometry, and scanning electron microscopy. The effects of reaction temperature, precipitant concentration, dripping speed of the salt solution, and the molar ratio of precipitant/total-cations on the composition, thermal behavior, and particle morphology of the resultant precursors were investigated. The precipitation conditions that yield carbonate precursors composed of ammonium dawsonite [NH4Al(OH)2CO3] and yttrium normal carbonate [Y2(CO3)3 · 3H2O] were determined.

Type
Articles
Information
Journal of Materials Research , Volume 15 , Issue 11 , November 2000 , pp. 2375 - 2386
Copyright
Copyright © Materials Research Society 2000

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