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Tribological and corrosion properties of AM70 magnesium alloy processed by equal channel angular pressing

Published online by Cambridge University Press:  08 May 2017

Karekere Rangaraju Gopi  and
Hanumanthappa Shivananda Nayaka
Karekere Rangaraju Gopi*
Affiliation:
Department of Mechanical Engineering, National Institute of Technology Karnataka, Surathkal 575025, India
Hanumanthappa Shivananda Nayaka
Affiliation:
Department of Mechanical Engineering, National Institute of Technology Karnataka, Surathkal 575025, India
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

Wear and corrosion properties of AM70 magnesium alloy subjected to equal channel angular pressing (ECAP) were investigated using pin-on-disc dry sliding wear test and electrochemical impedance spectroscopy (EIS), respectively. Wear test was conducted with 30 and 40 N loads with sliding distance of 5000 m and at a constant speed of 3 m/s. Reduced coefficient of friction (COF) and wear mass loss of ECAP processed samples showed increased wear resistance. Worn surface analysis by scanning electron microscope (SEM) showed the presence of delamination, wear debris, and plowing. Energy dispersive X-ray spectrometer (EDS) revealed the occurrence of oxidation, and the wear mechanism was identified as abrasion and oxidation wear. EIS plots showed the improvement in corrosion resistance of ECAP processed magnesium alloy compared to initial condition due to grain refinement and homogeneous distribution of secondary particles.

Keywords

equal channel angular pressingAM70 alloycoefficient of frictionelectrochemical impedance spectroscopyenergy dispersive X-ray spectrometerX-ray diffraction
Type
Articles
Information
Journal of Materials Research , Volume 32 , Issue 11 , 14 June 2017 , pp. 2153 - 2160
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Copyright
Copyright © Materials Research Society 2017 

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Footnotes

Contributing Editor: Jürgen Eckert

References

REFERENCES

Chen, Y.J., Wang, Q.D., Peng, J.G., Zhai, C.Q., and Ding, W.J.: Effects of extrusion ratio on the microstructure and mechanical properties of AZ31 Mg alloy. J. Mater. Process. Technol. 182, 281 (2007).CrossRefGoogle Scholar
Wu, G.F., Hu, H.J., Gong, X.B., Zhang, W.P., Wang, K.B., and Dong, T.X.: Application and development of casting process parameterized graph library based on AutoCAD software. Foundry Technol. 28, 535 (2007).Google Scholar
Kulekci, M.K.: Magnesium and its alloys applications in automotive industry. Int. J. Adv. Manuf. Technol. 39, 851 (2008).Google Scholar
Kojima, Y.: Handbook Advanced Mg Technology (Kallos Publishing Co. Ltd., Tokyo, 2000).Google Scholar
Gong, X., Li, H., Kang, S.B., Cho, J.H., and Li, S.: Microstructure and mechanical properties of twin-roll cast Mg–4.5Al–1.0Zn sheets processed by differential speed rolling. Mater. Des 31, 1581 (2010).Google Scholar
Gong, X., Kang, S.B., Li, S., and Cho, J.H.: Enhanced plasticity of twin-roll cast ZK60 magnesium alloy through differential speed rolling. Mater. Des. 30, 3345 (2009).CrossRefGoogle Scholar
Hoche, H., Blawert, C., Broszeit, E., and Berger, C.: Galvanic corrosion properties of differently PVD-treated magnesium die cast alloy AZ91. Surf. Coat. Technol. 193, 223 (2005).Google Scholar
Wang, R.M., Eliezer, A., and Gutman, E.M.: An investigation on the microstructure of an AM50 magnesium alloy. Mater. Sci. Eng., A 355, 201 (2003).Google Scholar
Du, X.N., Yin, S.M., Liu, S.C., Wang, B.Q., and Guo, J.D.: Effect of the electropulsing on mechanical properties and microstructure of an ECAPed AZ31 Mg alloy. J. Mater. Res. 23, 1570 (2008).Google Scholar
Wang, W., Wang, H., Liu, Y., Nie, H., and Cheng, W.: Effect of SiC nanoparticles addition on the microstructures and mechanical properties of ECAPed Mg9Al–1Si alloy. J. Mater. Res. 32, 615 (2017).CrossRefGoogle Scholar
Zhao, Y.H., Liao, X.Z., Zhu, Y.T., and Valiev, R.Z.: Enhanced mechanical properties in ultrafine grained 7075 Al alloy. J. Mater. Res. 20, 288 (2005).Google Scholar
Valiev, R.Z., Estrin, Y., Horita, Z., Langdon, T.G., Zechetbauer, M.J., and Zhu, Y.T.: Producing bulk ultrafine-grained materials by severe plastic deformation. JOM 58, 33 (2006).Google Scholar
Yang, Q. and Ghosh, A.K.: Deformation behavior of ultrafine-grain (UFG) AZ31B Mg alloy at room temperature. Acta Mater. 54, 5159 (2006).Google Scholar
Hu, H.J., Fan, J.Z., Wang, H., Zhai, Z.Y., Li, Y.Y., and Ou, Z.: Dry sliding wear behavior of ES-processed AZ31B magnesium alloy. Russ. J. Non-Ferr. Met. 56, 392 (2015).Google Scholar
Xu, J., Wang, X., Zhu, X., Shirooyeh, M., Wongsa-Ngam, J., Shan, D., Guo, B., and Langdon, T.G.: Dry sliding wear of an AZ31 magnesium alloy processed by equal-channel angular pressing. J. Mater. Sci. 48, 4117 (2013).CrossRefGoogle Scholar
Orlov, D., Ralston, K.D., Birbilis, N., and Estrin, Y.: Enhanced corrosion resistance of Mg alloy ZK60 after processing by integrated extrusion and equal channel angular pressing. Acta Mater. 59, 6176 (2011).Google Scholar
Minarik, P., Kral, R., and Janecek, M.: Effect of ECAP processing on corrosion resistance of AE21 and AE42 magnesium alloys. Appl. Surf. Sci. 281, 44 (2013).Google Scholar
Hadzima, B., Janecek, M., Bukovina, M., and Kral, R.: Electrochemical properties of fine-grained AZ31 magnesium alloy. Int. J. Mater. Res. 100, 1213 (2009).Google Scholar
Pardo, A., Merino, M.C., Coy, A.E., Arrabal, R., Viejo, F., and Matykina, E.: Corrosion behaviour of magnesium/aluminium alloys in 3.5 wt% NaCl. Corros. Sci. 50, 823 (2008).Google Scholar
Pardo, A., Merino, M.C., Coy, A.E., Viejo, F., Arrabal, R., and Feliu, S. Jr.: Influence of microstructure and composition on the corrosion behaviour of Mg/Al alloys in chloride media. Electrochim. Acta 53, 7890 (2008).Google Scholar
Kral, R., Minarik, P., Lesna, I.K., Skublova, L., Harcuba, P., Hadzima, B., and Janecek, M.: Effect of grain refinement on electrochemical characteristics in AE42 magnesium alloy. In WDS’11 Proceedings of Contributed Papers, Part III (2011); p. 136.Google Scholar
Jiang, J., Aibin, M.A., Saito, N., Zhixin, S.H.E.N., Dan, S.O.N.G., Fumin, L.U., Nishida, Y., Donghui, Y.A.N.G., and Pinghua, L.I.N.: Improving corrosion resistance of RE-containing magnesium alloy ZE41A through ECAP. J. Rare Earths 27, 848 (2009).Google Scholar
Gopi, K.R., Nayaka, H.S., and Sahu, S.: Investigation of microstructure and mechanical properties of ECAP-processed AM series magnesium alloy. J. Mater. Eng. Perform 25, 3737 (2016).CrossRefGoogle Scholar
Akbaripanah, F., Fereshteh-Saniee, F., Mahmudi, R., and Kim, H.K.: The influences of extrusion and equal channel angular pressing (ECAP) processes on the fatigue behavior of AM60 magnesium alloy. Mater. Sci. Eng., A 565, 308 (2013).Google Scholar
Li, P., Lei, M.K., and Zhu, X.P.: Dry sliding tribological behavior of AZ31 magnesium alloy irradiated by high-intensity pulsed ion beam. Appl. Surf. Sci. 257, 72 (2010).Google Scholar
Archard, J.: Contact and rubbing of flat surfaces. J. Appl. Phys. 24, 981 (1953).Google Scholar
Taltavull, C., Rodrigo, P., Torres, B., Lopez, A.J., and Rams, J.: Dry sliding wear behavior of AM50B magnesium alloy. Mater. Des. 56, 549 (2014).CrossRefGoogle Scholar
Cao, C.: On the impedance plane displays for irreversible electrode reactions based on the stability conditions of the steady-state-I. One state variable besides electrode potential. Electrochim. Acta 35, 831 (1990).Google Scholar
Song, D., Ma, A., Jiang, J., Lin, P., Yang, D., and Fan, J.: Corrosion behavior of equal-channel-angular-pressed pure magnesium in NaCl aqueous solution. Corros. Sci. 52, 481 (2010).Google Scholar
Song, D., Ma, A.B., Jiang, J.H., Lin, P.H., Yang, D.H., and Fan, J.F.: Corrosion behaviour of bulk ultra-fine grained AZ91D magnesium alloy fabricated by equal-channel angular pressing. Corros. Sci. 53, 362 (2011).Google Scholar
Ralston, K.D. and Birbilis, N.: Effect of grain size on corrosion: A review. Corrosion 66, 075005 (2010).Google Scholar
Song, G.: Recent progress in corrosion and protection of magnesium alloys. Adv. Eng. Mater. 7, 563 (2005).Google Scholar
Johansen, N.A., Adams, G.B., and Van Rysselberghe, P.: Anodic oxidation of aluminum, chromium, hafnium, tantalum, titanium, vanadium, and zirconium at very low current densities. J. Electrochem. Soc. 104, 339 (1957).CrossRefGoogle Scholar
Wang, L., Shinohara, T., and Zhang, B.P.: Corrosion behavior of AZ31 magnesium alloy in dilute sodium chloride solutions. Zairyo-to-Kankyo 58, 105 (2009).Google Scholar