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Preparation of textured alumina films by the sol-gel route

Published online by Cambridge University Press:  03 March 2011

J. Campaniello
Affiliation:
Laboratoire de Chimie des Solides, URA 446-CNRS, Bât. 414, Université Paris Sud, 91405 Orsay Cedex, France
P. Berthet*
Affiliation:
Laboratoire de Chimie des Solides, URA 446-CNRS, Bât. 414, Université Paris Sud, 91405 Orsay Cedex, France
F. d'Yvoire
Affiliation:
Laboratoire de Chimie des Solides, URA 446-CNRS, Bât. 414, Université Paris Sud, 91405 Orsay Cedex, France
A. Revcolevschi
Affiliation:
Laboratoire de Chimie des Solides, URA 446-CNRS, Bât. 414, Université Paris Sud, 91405 Orsay Cedex, France
*
a)Author to whom correspondence should be addressed.
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Abstract

Alumina films were fabricated by the sol-gel route under various preparation conditions. The peptization rate and the structure of colloidal particles depend on these conditions. In particular, the peptization of a dried boehmite precipitate prepared from aluminum alkoxide was achieved within a few seconds without heating. The resulting sol is made of highly dispersed crystallites; this allows the formation of well-textured xerogel films as evidenced by the Weissenberg x-ray method.

Type
Articles
Copyright
Copyright © Materials Research Society 1995

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References

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