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Microstructural development and room temperature tensile property of directionally solidified Ti–47Al alloys by electromagnetic confinement and directional solidification

Published online by Cambridge University Press:  27 April 2018

Yujun Du*
Affiliation:
State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China
Jun Shen*
Affiliation:
State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China
Yilong Xiong
Affiliation:
State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China
Zhao Shang
Affiliation:
State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China
Ling Qin
Affiliation:
State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China
Hengzhi Fu
Affiliation:
State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi’an 710072, China
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

Ti–47Al samples with a diameter of 18 mm are obtained by electromagnetic confinement and directional solidification at different growth velocities. Controlled by a Ti–43Al–3Si seed, the α grains are aligned well and the parallel lamellar microstructure is obtained at the growth velocity of 10 μm/s. With the growth velocity increases to 25 and 50 μm/s, although the lamellar microstructures are still aligned well in the initial transition stage, the lamellar alignment fails due to the nucleation and growth of new β and α grains and then the inclined and perpendicular lamellar microstructures form eventually. The room temperature tensile properties of the different lamellar microstructures are measured and the results show that the desired lamellar microstructure has a tensile strength of 693 MPa and an elongation of 10.0% simultaneously. They are the maximum values that have been reported in binary γ-TiAl alloys so far and are far higher than those of the other two types of lamellar microstructures. The fracture behaviors of the lamellar microstructures are checked by scanning electron microscopy and transmission electron microscopy. Two models are used to illustrate the fracture mechanism of the different lamellar structures.

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Article
Copyright
Copyright © Materials Research Society 2018 

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Footnotes

Contributing Editor: Jürgen Eckert

References

REFERENCES

Kothari, K., Radhakrishnan, R., and Wereley, N.M.: Advances in gamma titanium aluminides and their manufacturing techniques. Prog. Aeronaut. Sci. 55, 1 (2012).CrossRefGoogle Scholar
Kim, S., Hong, J.K., Na, Y., Yeom, J., and Kim, S.E.: Development of TiAl alloys with excellent mechanical properties and oxidation resistance. Mater. Des. 54, 814 (2014).CrossRefGoogle Scholar
Ding, J., Zhang, M., Ye, T., Liang, Y., Ren, Y., Dong, C., and Lin, J.: Microstructure stability and micro-mechanical behavior of as-cast gamma-TiAl alloy during high-temperature low cycle fatigue. Acta Mater. 145, 504 (2018).CrossRefGoogle Scholar
Yamaguchi, M., Inui, H., and Ito, K.: High-temperature structural intermetallics. Acta Mater. 48, 307 (2000).CrossRefGoogle Scholar
Inui, H., Oh, M.H., Nakamura, A., and Yamaguchi, M.: Room-temperature tensile deformation of polysynthetically twinned (PST) crystals of TiAl. Acta Metall. Mater. 40, 3095 (1992).CrossRefGoogle Scholar
Wang, Q., Ding, H., Zhang, H., Chen, R., Guo, J., and Fu, H.: Influence of Mn addition on the microstructure and mechanical properties of a directionally solidified γ-TiAl alloy. Mater. Charact. 137, 133 (2018).CrossRefGoogle Scholar
Du, Y.J., Shen, J., Xiong, Y.L., Shang, Z., and Fu, H.Z.: Stability of lamellar microstructures in a Ti–48Al–2Nb–2Cr alloy during heat treatment and its application to lamellae alignment as a quasi-seed. Intermetallics 61, 80 (2015).CrossRefGoogle Scholar
Johnson, D.R., Inui, H., Muto, S., Omiya, Y., and Yamanaka, T.: Microstructural development during directional solidification of α-seeded TiAl alloys. Acta Mater. 54, 1077 (2006).CrossRefGoogle Scholar
Nie, G., Ding, H.S., Chen, R.R., Guo, J.J., and Fu, H.Z.: Microstructural control and mechanical properties of Ti–47Al–2Cr–2Nb alloy by directional solidification electromagnetic cold crucible technique. Mater. Des. 39, 350 (2012).CrossRefGoogle Scholar
Ding, X.F., Lin, J.P., Zhang, L.Q., Su, Y.Q., and Chen, G.L.: Microstructural control of TiAl–Nb alloys by directional solidification. Acta Mater. 60, 498 (2012).CrossRefGoogle Scholar
Johnson, D.R., Inui, H., and Yamaguchi, M.: Directional solidification and microstructural control of the TiAl/Ti3Al lamellar microstructure in TiAl–Si alloys. Acta Mater. 44, 2523 (1996).CrossRefGoogle Scholar
Du, Y.J., Shen, J., Xiong, Y.L., Shang, Z., Wang, L., and Fu, H.Z.: Lamellar microstructure alignment and fracture toughness in Ti–47Al alloy by electromagnetic confinement and directional solidification. Mater. Sci. Eng., A 621, 94 (2015).CrossRefGoogle Scholar
Ding, X.F., Zhang, L.Q., Lin, J.P., He, J.P., Yin, J., and Chen, G.L.: Microstructure control and mechanical properties of directionally solidified TiAl–Nb alloys. Trans. Nonferrous Met. Soc. 22, 747 (2012).CrossRefGoogle Scholar
Luo, W.Z., Shen, J., Min, Z.X., and Fu, H.Z.: Investigation of interfacial reactions between TiAl alloy and crucible materials during directional solidification process. Rare Met. Mater. Eng 38, 1441 (2009).Google Scholar
Lee, H.N., Johnson, D.R., Inui, H., Oh, M.H., Wee, D.M., and Yamaguchi, M.: Microstructural control through seeding and directional solidification of TiAl alloys containing Mo and C. Acta Mater. 48, 3221 (2000).CrossRefGoogle Scholar
Takeyama, M., Yamamoto, Y., Morishima, H., Koike, K., Chang, S.Y., and Matsuo, T.: Lamellar orientation control of Ti–48Al PST crystal by unidirectional solidification. Mater. Sci. Eng., A 329–331, 7 (2002).CrossRefGoogle Scholar
Zheng, X.Q., Shen, J., Ding, H.S., Chen, R.R., and Xu, X.: Preparation of fully lamellar microstructure Ti–43Al–3Si alloy with alignment perpendicular to the growth direction in steel mould. Mater. Rev. 19, 118 (2005).Google Scholar
Tiller, W.A., Jackson, K.A., Rutter, J.W., and Chalmers, B.: The redistribution of solute atoms during the solidification of metals. Acta Metall. 1, 428 (1953).CrossRefGoogle Scholar
Hunziker, O., Vandyoussefi, M., and Kurz, W.: Phase and microstructure selection in peritectic alloys close to the limit of constitutional undercooling. Acta Mater. 46, 6325 (1998).CrossRefGoogle Scholar
Wang, L.S., Shen, J., Xiong, Y.L., Du, Y.J., and Fu, H.Z.: Phase and microstructure selection during directional solidification of peritectic alloy under convection condition. Acta Metall. Sin. 27, 585 (2014).CrossRefGoogle Scholar
Li, X.Z., Sun, T., Yu, C.X., Su, Y.Q., Cao, Y.Z., Guo, J.J., and Fu, H.Z.: Solidification phase selection in directionally solidified Ti–(44–54%)Al alloys. Acta Metall. Sin. 45, 1479 (2009).Google Scholar
Du, Y.J., Shen, J., Xiong, Y.L., Liu, Z.W., Zhao, Q., and Fu, H.Z.: Determining the effects of growth velocity on microstructure and mechanical properties of Ti–47Al alloy using electromagnetic confinement and directional solidification. JOM 66, 1914 (2014).CrossRefGoogle Scholar
Luo, W.Z., Shen, J., Min, Z.X., and Fu, H.Z.: Lamellar orientation control of TiAl alloys under high temperature gradient with a Ti–43Al–3Si seed. J. Cryst. Growth 310, 5441 (2008).CrossRefGoogle Scholar
Ding, H.S., Nie, G., Chen, R.R., Guo, J.J., and Fu, H.Z.: High temperature deformation behaviors of polysynthetically twinned (PST) Ti–47Al–2Cr–2Nb alloy. Mater. Sci. Eng., A 558, 747 (2012).Google Scholar
Hwu, K.L. and Derby, B.: Fracture of metal/ceramic laminates—I. Transition from single to multiple cracking. Acta Mater. 47, 529 (1999).CrossRefGoogle Scholar
Zambaldi, C. and Raabe, D.: Plastic anisotropy of γ-TiAl revealed by axisymmetric indentation. Acta Mater. 58, 3516 (2010).CrossRefGoogle Scholar
Meyers, M.A.E.: Mechanical Behavior of Materials, 2nd ed. (Cambridge University Press, Cambridge, U.K., 2009); p. 470.Google Scholar