Hostname: page-component-586b7cd67f-r5fsc Total loading time: 0 Render date: 2024-11-28T08:15:59.807Z Has data issue: false hasContentIssue false
  • English
  • Français

Grain refining and improving mechanical properties of AZ31 Mg alloy sheets by multi-pass warm rolling with falling temperature

Published online by Cambridge University Press:  03 September 2018

Yanchun Zhao ,
Hua Zhang ,
Jianfeng Fan ,
Lifei Wang ,
Qiang Zhang ,
Cheng Peng ,
Hongbiao Dong  and
Bingshe Xu
Yanchun Zhao
Affiliation:
Department of Materials Science and Engineering, Yangze Normal University, Chongqing 408100, China
Hua Zhang*
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Research Center of Advanced Materials Science and Technology, Taiyuan University of Technology, Taiyuan 030024, China
Jianfeng Fan
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Research Center of Advanced Materials Science and Technology, Taiyuan University of Technology, Taiyuan 030024, China
Lifei Wang
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Research Center of Advanced Materials Science and Technology, Taiyuan University of Technology, Taiyuan 030024, China
Qiang Zhang*
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Research Center of Advanced Materials Science and Technology, Taiyuan University of Technology, Taiyuan 030024, China
Cheng Peng
Affiliation:
Department of Materials Science and Engineering, Yangze Normal University, Chongqing 408100, China
Hongbiao Dong
Affiliation:
Department of Engineering, University of Leicester, Leicester LE1 7RH, U.K.
Bingshe Xu
Affiliation:
Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Research Center of Advanced Materials Science and Technology, Taiyuan University of Technology, Taiyuan 030024, China
*
a)Address all correspondence to this author. e-mail: [email protected]
Get access

Abstract

Multi-pass warm rolling with falling temperature was proposed and investigated to obtain AZ31 Mg alloy sheets with a fine-grained microstructure. The results indicated that the grain microstructure of AZ31 alloy sheets was successfully refined from 22.1 to 4.5 μm after multi-pass warm rolling with falling temperature and annealing. Compared to the as-received sheet, the multi-pass warm rolled sheets in annealed condition exhibited weaker (0001) basal texture intensity, which resulted in the significantly increased Schmid factor of 〈a〉 basal slip. After multi-pass warm rolling with falling temperature, the rolled sheets in annealed condition also exhibited much better mechanical properties, e.g., higher tensile strength, larger fracture elongation, and higher Erichsen value, especially the IE of 8-pass warm rolled sheet in annealed condition was significantly increased by ∼33% under the same thickness, which could be attributed to the refined grain microstructure and the weakened basal texture.

Keywords

AZ31 Mg alloymulti-pass warm rollingmicrostructuregrain refiningmechanical property
Type
Article
Information
Journal of Materials Research , Volume 33 , Issue 18 , 28 September 2018 , pp. 2827 - 2834
Copyright
Copyright © Materials Research Society 2018 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

Li, J.C., He, Z.L., Fu, P.H., Wu, Y.J., Peng, L.M., and Ding, W.J.: Heat treatment and mechanical properties of a high-strength cast Mg–Gd–Zn alloy. Mater. Sci. Eng. A 651, 745 (2016).CrossRefGoogle Scholar
Cui, W.D., Xiao, L., Liu, W.C., Wu, G.H., Wang, X.F., and Li, Z.Q.: Effect of Zn addition on microstructure and mechanical properties of Mg–9Gd–3Y–0.5Zr alloy. J. Mater. Res. 33, 733 (2018).CrossRefGoogle Scholar
Pan, F.S., Zeng, B., iang, B., Zhang, M.X., and Dong, H.W.: Enhanced mechanical properties of AZ31B magnesium alloy thin sheets processed by on-line heating rolling. J. Alloys Compd. 693, 414 (2017).CrossRefGoogle Scholar
Zhang, C.Z., Guan, S.K., Wang, L.G., Zhu, S.J., and Chang, L.: The microstructure and corrosion resistance of biological Mg–Zn–Ca alloy processed by high-pressure torsion and subsequently annealing. J. Mater. Res. 32, 1061 (2017).CrossRefGoogle Scholar
He, J.J., Jiang, B., Yua, X.W., Xu, J., Jiang, Z.T., Liu, B., and Pan, F.S.: Strain path dependence of texture and property evolutions on rolled Mg–Li–Al–Zn alloy possessed of an asymmetric texture. J. Alloys Compd. 698, 771 (2017).CrossRefGoogle Scholar
Cheng, W.L., Wang, L.F., Zhang, H., and Cao, X.Q.: Enhanced stretch formability of AZ31 magnesium alloy thin sheet by pre-crossed twinning lamellas induced static recrystallizations. J. Mater. Process. Technol. 254, 302 (2018).CrossRefGoogle Scholar
Styczynski, A., Hartig, C., Bohlen, J., and Letzig, D.: Cold rolling textures in AZ31 wrought magnesium alloy. Scr. Mater. 50, 943 (2003).CrossRefGoogle Scholar
Yua, D.L., Zhang, D.F., Sun, J., Luo, Y.X., Xua, J.Y., Zhang, H.J., and Pan, F.S.: Improving mechanical properties of ZM61 magnesium alloy by aging before extrusion. J. Alloys Compd. 690, 553 (2017).CrossRefGoogle Scholar
Yi, S.B., Bohlen, J., Heinemann, F., and Letzig, D.: Mechanical anisotropy and deep drawing behaviour of AZ31 and ZE10 magnesium alloy sheets. Acta Mater. 58, 592 (2010).CrossRefGoogle Scholar
Iwanaga, K., Tashiro, H., Okamoto, H., and Shimizu, K.: Improvement of formability from room temperature to warm temperature in AZ-31 magnesium alloy. J. Mater. Process. Technol. 155–156, 1313 (2004).CrossRefGoogle Scholar
Suh, J., Victoria-Hernández, J., Letzig, D., Golle, R., and Volk, W.: Effect of processing route on texture and cold formability of AZ31 Mg alloy sheets processed by ECAP. Mater. Sci. Eng. A 669, 159 (2016).CrossRefGoogle Scholar
Mironov, S., Onuma, T., Sato, Y.S., Yoneyama, S., and Kokawa, H.: Tensile behavior of friction-stir welded AZ31 magnesium alloy. Mater. Sci. Eng. A 679, 272 (2017).CrossRefGoogle Scholar
Vargas, M., Lathabai, S., Uggowitzer, P.J., Qi, Y., Orlov, D., and Estrind, Y.: Microstructure, crystallographic texture and mechanical behaviour of friction stir processed Mg–Zn–Ca–Zr alloy ZKX50. Mater. Sci. Eng. A 685, 253 (2017).CrossRefGoogle Scholar
Kaseem, M., Chung, B.K., Yang, H.W., Hamad, K., and Ko, Y.G.: Effect of deformation temperature on microstructure and mechanical properties of AZ31 Mg alloy processed by differential-speed rolling. J. Mater. Sci. Technol. 31, 498 (2015).CrossRefGoogle Scholar
Luo, D., Wang, H.Y., Zhao, L.G., Wang, C., Liu, G.J., Liu, Y., and Jiang, Q.C.: Effect of differential speed rolling on the room and elevated temperature tensile properties of rolled AZ31 Mg alloy sheets. Mater. Charact. 124, 223 (2017).CrossRefGoogle Scholar
Wang, Q.D., Mu, Y.L., Lin, J.B., Zhang, L., and Roven, H.J.: Strengthening and toughening mechanisms of an ultrafine grained Mg–Gd–Y–Zr alloy processed by cyclic extrusion and compression. Mater. Sci. Eng. A 699, 26 (2017).CrossRefGoogle Scholar
Tian, Y., Huang, H., Yuan, G.Y., and Ding, W.J.: Microstructure evolution and mechanical properties of quasicrystal-reinforced Mg–Zn–Gd alloy processed by cyclic extrusion and compression. J. Alloys Compd. 626, 42 (2015).CrossRefGoogle Scholar
Liu, H., Ju, J., Lu, F.M., Yan, J.L., Bai, J., Jiang, J.H., and Ma, A.B.: Dynamic precipitation behavior and mechanical property of an Mg94Y4Zn2 alloy prepared by multi-passes successive equal channel angular pressing. Mater. Sci. Eng. A 682, 255 (2017).CrossRefGoogle Scholar
Motoyama, T., Watanabe, H., Ikeo, N., and Mukai, T.: Mechanical and damping properties of equal channel angular extrusion-processed Mg–Ca alloys. Mater. Lett. 201, 144 (2017).CrossRefGoogle Scholar
Tang, Y., Le, Q.C., Jia, W.T., Liu, X., and Cui, J.Z.: Influences of warm rolling and annealing processes on microstructure and mechanical properties of three parent structures containing Mg–Li alloys. Mater. Sci. Eng. A 711, 1 (2018).CrossRefGoogle Scholar
Jia, W.P., Hu, X.D., Zhao, H.Y., Ju, D.Y., and Chen, D.L.: Texture evolution of AZ31 magnesium alloy sheets during warm rolling. J. Alloys Compd. 645, 70 (2015).CrossRefGoogle Scholar
Liu, D., Liu, Z.Y., and Wang, E.: Effect of rolling reduction on microstructure, texture, mechanical properties and mechanical anisotropy of AZ31 magnesium alloys. Mater. Sci. Eng. A 612, 208 (2014).CrossRefGoogle Scholar
Yu, Z.P., Yan, Y.H., Yao, J., Wang, C., Zha, M., Xu, X.Y., Liu, Y., Wang, H.Y., and Jiang, Q.C.: Effect of tensile direction on mechanical properties and microstructural evolutions of rolled Mg–Al–Zn–Sn magnesium alloy sheets at room and elevated temperatures. J. Alloys Compd. 744, 211 (2018).CrossRefGoogle Scholar
Huang, X.S., Suzuki, K., Chino, Y., and Mabuchi, M.: Texture and stretch formability of AZ61 and AM60 magnesium alloy sheets processed by high-temperature rolling. J. Alloys Compd. 632, 94 (2015).CrossRefGoogle Scholar
Chen, W.Z., Zhang, W.C., Zhang, L.X., and Wang, E.D.: Property improvements in fine-grained Mg–Zn–Zr alloy sheets produced by temperature-step-down multi-pass rolling. J. Alloys Compd. 646, 195 (2015).CrossRefGoogle Scholar
Li, X., Yang, P., Wang, L.N., Meng, L., and Cui, F.: Orientational analysis of static recrystallization at compression twins in a magnesium alloy AZ31. Mater. Sci. Eng. A 517, 160 (2009).CrossRefGoogle Scholar
Myshlyaev, M.M., McQueen, H.J., Mwembela, A., and Konopleva, E.: Twinning, dynamic recovery and recrystallization in hot worked Mg–Al–Zn alloy. Mater. Sci. Eng. A 337, 121 (2002).CrossRefGoogle Scholar
Suzuki, M., Sato, H., Maruyama, K., and Oikawa, H.: Creep deformation behavior and dislocation substructures of Mg–Y binary alloys. Mater. Sci. Eng., A 319–321, 751 (2001).CrossRefGoogle Scholar
Huang, X., Suzuki, K., and Chino, Y.: Annealing behaviour of Mg–3Al–1Zn alloy sheet obtained by a combination of high-temperature rolling and subsequent warm rolling. J. Alloys Compd. 509, 4854 (2011).CrossRefGoogle Scholar
Chino, Y., Kimura, K., and Mabuchi, M.: Twinning behavior and deformation mechanisms of extruded AZ31 Mg alloy. Mater. Sci. Eng. A 483, 481 (2008).CrossRefGoogle Scholar
Yang, Q.S., Jiang, B., Zhou, G.Y., Dai, J.H., and Pan, F.S.: Influence of an asymmetric shear deformation on microstructure evolution and mechanical behavior of AZ31 magnesium alloy sheet. Mater. Sci. Eng. A 590, 440 (2014).CrossRefGoogle Scholar
Brown, D.W., Agnew, S.R., Bourke, M.A.M., Holden, T.M., Vogel, S.C., and Tomé, C.N.: Internal strain and texture evolution during deformation twinning in magnesium. Mater. Sci. Eng. A 399, 1 (2005).CrossRefGoogle Scholar
Zhang, H., Cheng, W.L., Fan, J.F., Xu, B.S., and Dong, H.B.: Improved mechanical properties of AZ31 magnesium alloy sheets by repeated cold rolling and annealing using a small pass reduction. Mater. Sci. Eng. A 637, 243 (2015).CrossRefGoogle Scholar
Agnew, S.R. and Duygulu, O.: A mechanistic understanding of the formability of magnesium: Examining the role of temperature on the deformation mechanisms. Mater. Sci. Forum 419–422, 177 (2003).CrossRefGoogle Scholar
Agnew, S.R. and Duygulu, O.: Plastic anisotropy and the role of non-basal slip in magnesium alloy AZ31B. Int. J. Plast. 21, 1161 (2005).CrossRefGoogle Scholar
del Valle, J.A., Carreño, F., and Ruano, O.A.: Influence of texture and grain size on work hardening and ductility in magnesium-based alloys processed by ECAP and rolling. Acta Mater. 54, 4247 (2006).CrossRefGoogle Scholar
Yuan, W. and Mishra, R.S.: Grain size and texture effects on deformation behavior of AZ31 magnesium alloy. Mater. Sci. Eng. A 558, 716 (2012).CrossRefGoogle Scholar
Zhang, H., Huang, G.S., Wang, L.F., and Li, J.H.: Improved formability of Mg–3Al–1Zn alloy by pre-stretching and annealing. Scr. Mater. 67, 495 (2012).CrossRefGoogle Scholar
Koike, J., Kobayashi, T., Mukai, T., Watanabe, H., Suzuki, M., Maruyama, K., and Higashi, K.: The activity of non-basal slip systems and dynamic recovery at room temperature in fine-grained AZ31B magnesium alloys. Acta Mater. 51, 2055 (2003).CrossRefGoogle Scholar
Barnett, M.R.: Twinning and the ductility of magnesium alloys: Part I: “Tension” twins. Mater. Sci. Eng. A 464, 1 (2007).CrossRefGoogle Scholar
Barnett, M.R.: Twinning and the ductility of magnesium alloys: Part II. “Contraction” twins. Mater. Sci. Eng. A 464, 8 (2007).CrossRefGoogle Scholar