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Conventional Vickers and true instrumented indentation hardness determined by instrumented indentation tests

Published online by Cambridge University Press:  31 January 2011

Seung-Kyun Kang ,
Ju-Young Kim ,
Chan-Pyoung Park ,
Hyun-Uk Kim  and
Dongil Kwon
Seung-Kyun Kang
Affiliation:
Department of Materials Science and Engineering, Seoul National University, Seoul 151-744, Korea
Ju-Young Kim*
Affiliation:
Materials Science, California Institute of Technology, Pasadena, California 91106
Dongil Kwon
Affiliation:
Department of Materials Science and Engineering, Seoul National University, Seoul 151-744, Korea
*
a)Address all correspondence to this author. e-mail: [email protected]
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Abstract

We evaluate Vickers hardness and true instrumented indentation test (IIT) hardness of 24 metals over a wide range of mechanical properties using just IIT parameters by taking into account the real contact morphology beneath the Vickers indenter. Correlating the conventional Vickers hardness, indentation contact morphology, and IIT parameters for the 24 metals reveals relationships between contact depths and apparent material properties. We report the conventional Vickers and true IIT hardnesses measured only from IIT contact depths; these agree well with directly measured hardnesses within ±6% for Vickers hardness and ±10% for true IIT hardness.

Keywords

HardnessMetalSteel
Type
Articles
Information
Journal of Materials Research , Volume 25 , Issue 2 , February 2010 , pp. 337 - 343
Copyright
Copyright © Materials Research Society 2010

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References

REFERENCES

1.Bulychev, S.I., Alekhin, V.P., Shorshorov, M.K., Ternovskii, A.P., Shnyrev, G.D.Determining Young's modulus from the indentor penetration diagram. Zavod. Lab. 41, 1137 (1975)Google Scholar
2.Doerner, M.F., Nix, W.D.A method for interpreting the data from depth-sensing indentation instruments. J. Mater. Res. 1, 601 (1986)CrossRefGoogle Scholar
3.Oliver, W.C., Pharr, G.M.An improved technique for determining hardness and elastic-modulus using load and displacement sensing indentation experiments. J. Mater. Res. 7, 1564 (1992)CrossRefGoogle Scholar
4.Gouldstone, A., Chollacoop, N., Dao, M., Li, J., Minor, A.M., Shen, Y.L.Indentation across size scales and disciplines: Recent developments in experimentation and modeling. Acta Mater. 55, 4015 (2007)CrossRefGoogle Scholar
5.Fischer-Cripps, A.C.A review of analysis methods for sub-micron indentation testing. Vacuum 58, 569 (2000)CrossRefGoogle Scholar
6.Mukhopadhyay, N.K., Paufler, P.Micro- and nanoindentation techniques for mechanical characterisation of materials. Int. Mater. Rev. 51, 209 (2006)CrossRefGoogle Scholar
7.Field, J.S., Swain, M.V.Determining the mechanical-properties of small volumes of material from submicrometer spherical indentations. J. Mater. Res. 10, 101 (1995)CrossRefGoogle Scholar
8.Schuh, C.A.Nanoindentation studies of materials. Mater. Today 9, 32 (2006)CrossRefGoogle Scholar
9.Tabor, D.Hardness of Metals (Clarendon Press, Oxford 1951)Google Scholar
10.Bolshakov, A., Pharr, G.M.Influences of pileup on the measurement of mechanical properties by load and depth-sensing indentation techniques. J. Mater. Res. 13, 1049 (1998)CrossRefGoogle Scholar
11.Fischer-Cripps, A.C.Nanoindentation (Springer, New York 2002)CrossRefGoogle Scholar
12.Oliver, W.C., Pharr, G.M.Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology. J. Mater. Res. 19, 3 (2004)CrossRefGoogle Scholar
13.Cheng, Y.T., Cheng, C.M.Scaling, dimensional analysis, and indentation measurements. Mater. Sci. Eng., R 44, 91 (2004)CrossRefGoogle Scholar
14.Kim, J.Y., Kang, S.K., Greer, J.R., Kwon, D.Evaluating plastic flow properties by characterizing indentation size effect using a sharp indenter. Acta Mater. 56, 3338 (2008)CrossRefGoogle Scholar
15.Kim, J.Y., Kang, S.K., Lee, J.J., Jang, J.I., Lee, Y.H., Kwon, D.Influence of surface-roughness on indentation size effect. Acta Mater. 55, 3555 (2007)CrossRefGoogle Scholar
16.Ahn, J.H., Kwon, D.Derivation of plastic stress–strain relationship from ball indentations: Examination of strain definition and pileup effect. J. Mater. Res. 16, 3170 (2001)CrossRefGoogle Scholar
17.Kim, S.H., Lee, B.W., Choi, Y., Kwon, D.Quantitative determination of contact depth during spherical indentation of metallic materials—A FEM study. Mater. Sci. Eng., A 415, 59 (2006)CrossRefGoogle Scholar
18.Kim, J.Y., Lee, K.W., Lee, J.S., Kwon, D.Determination of tensile properties by instrumented indentation technique: Representative stress and strain approach. Surf. Coat. Technol. 201, 4278 (2006)CrossRefGoogle Scholar
19.Jeon, E.C., Kim, J.Y., Baik, M.K., Kim, S.H., Park, J.S., Kwon, D.Optimum definition of true strain beneath a spherical indenter for deriving indentation flow curves. Mater. Sci. Eng., A 419, 196 (2006)CrossRefGoogle Scholar
20.Taljat, B., Zacharia, T., Kosel, F.New analytical procedure to determine stress–strain curve from spherical indentation data. Int. J. Solids Struct. 35, 4411 (1998)CrossRefGoogle Scholar
21.Dao, M., Chollacoop, N., Van Vliet, K.J., Venkatesh, T.A., Suresh, S.Computational modeling of the forward and reverse problems in instrumented sharp indentation. Acta Mater. 49, 3899 (2001)CrossRefGoogle Scholar
22.Chollacoop, N., Dao, M., Suresh, S.Depth-sensing instrumented indentation with dual sharp indenters. Acta Mater. 51, 3713 (2003)CrossRefGoogle Scholar
23.Herbert, E.G., Pharr, G.M., Oliver, W.C., Lucas, B.N., Hay, J.L.On the measurement of stress–strain curves by spherical indentation. Thin Solid Films 398–399, 331 (2001)CrossRefGoogle Scholar
24.Jayaraman, S., Hahn, G.T., Oliver, W.C., Rubin, C.A., Bastias, P.C.Determination of monotonic stress–strain curve of hard materials from ultra-low-load indentation tests. Int. J. Solids Struct. 35, 365 (1998)CrossRefGoogle Scholar
25.Cheng, Y.T., Cheng, C.M.Scaling relationships in conical indentation of elastic perfectly plastic solids. Int. J. Solids Struct. 36, 1231 (1999)CrossRefGoogle Scholar
26.Giannakipoulos, A.E., Suresh, S.Determination of elastoplastic properties by instrumented sharp indentation. Scr. Mater. 40, 1191 (1999)CrossRefGoogle Scholar
27.Venkatesh, T.A., Van Vliet, K.J., Giannakopoulos, A.E., Suresh, S.Determination of elasto-plastic properties by instrumented sharp indentation: Guidelines for property extraction. Scr. Mater. 42, 833 (2000)CrossRefGoogle Scholar
28.Bucaille, J.L., Stauss, S., Felder, E., Michler, J.Determination of plastic properties of metals by instrumented indentation using different sharp indenters. Acta Mater. 51, 1663 (2003)CrossRefGoogle Scholar
29.Bouzakis, K.D., Michailidis, N.Coating elastic-plastic properties determined by means of nanoindentations and FEM-supported evaluation algorithms. Thin Solid Films 469–470, 227 (2004)CrossRefGoogle Scholar
30.Cheng, Y.T., Cheng, C.M.Relationships between hardness, elastic modulus, and the work of indentation. Appl. Phys. Lett. 73, 614 (1998)CrossRefGoogle Scholar
31.Cheng, Y.T., Cheng, C.M.What is indentation hardness? Surf. Coat. Technol. 133–134, 417 (2000)CrossRefGoogle Scholar
32.Malzbendera, J., de With, G.Indentation load–displacement curve, plastic deformation, and energy. J. Mater. Res. 17, 502 (2002)CrossRefGoogle Scholar
33.McElhaney, K.W., Vlassak, J.J., Nix, W.D.Determination of indenter tip geometry and indentation contact area for depth-sensing indentation experiments. J. Mater. Res. 13, 1300 (1998)CrossRefGoogle Scholar
34.Mencik, J., Swain, M.V.Error associated with depth sensing micro-indentation. J. Mater. Res. 10, 1491 (1995)CrossRefGoogle Scholar
35.Alcala, J., Barone, A.C., Anglada, M.The influence of plastic hardening on surface deformation modes around Vickers and spherical indents. Acta Mater. 48, 3451 (2000)CrossRefGoogle Scholar
36.Choi, Y., Lee, H.S., Kwon, D.Analysis of sharp-tip-indentation load-depth curve for contact area determination taking into account pile-up and sink-in effects. J. Mater. Res. 19, 3307 (2004)CrossRefGoogle Scholar
37.Lee, Y.H., Hahn, J.H., Nahm, S.H., Jang, J.I., Kwon, D.Investigations on indentation size effects using a pile-up corrected hardness. J. Phys. D: Appl. Phys. 41, 074027 (2008)CrossRefGoogle Scholar
38.ISO/FDIS 14577-1 Metallic Materials—Instrumented Indentation Test for Hardness and Materials Parameters; Part 1, Test Method (International Organization for Standardization, Geneva, Switzerland 2002)Google Scholar
39.ASTM E8-04 Standard Test Methods for Tension Testing of Metallic Materials (ASTM International, W, Conshohocken, PA 2002)Google Scholar