Hostname: page-component-586b7cd67f-rcrh6 Total loading time: 0 Render date: 2024-11-28T06:40:03.805Z Has data issue: false hasContentIssue false
  • English
  • Français

Scanning X-Ray Analytical Microscope using X-Ray Guide Tube

Published online by Cambridge University Press:  06 March 2019

Shuichi Shimomura  and
Hiromoto Nakazawa
Shuichi Shimomura
Affiliation:
National Institute for Research in Inorganic Materials 1-1 Namiki, Tsukuba-shi, Ibaraki-ken, 305 Japan
Hiromoto Nakazawa
Affiliation:
National Institute for Research in Inorganic Materials 1-1 Namiki, Tsukuba-shi, Ibaraki-ken, 305 Japan
Get access

Abstract

A scanning X-ray analytical microscope was constructed using X-ray guide tube(XGT). XGT is a glass capillary which guides and focuses x-rays by total external reflection at the inner wall. The nature of X-ray beam passed through XGT is varied depending on the form of XGT. The cylindrical and conical types were used for the present setup. A small area (10μm × 10μm) of the sample was irradiated by the X-ray microbeam formed by XGT. Fluorescent and diffracted X-rays from the small area were detected by SSD. By scanning the sample in the plane normal to the X-ray microbeam, the intensity distributions of such secondary x-rays were measured and used as picture elements for constructing x-ray mapping images. The sample was a thin-section of an old chinaware. The images suggest a wide application of this instrument.

Type
XV. X-Ray Imaging and Tomography
Information
Advances in X-Ray Analysis , Volume 35 , Issue B: First Pacific-International Congress on X-ray Analytical Methods (PICXAM). Fortieth Annual Conference on Applications of X-ray Analysis, August 7-16, 1991 , 1991 , pp. 1289 - 1293
Copyright
Copyright © International Centre for Diffraction Data 1991

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Hakazawa, H., J. Appl. Cryst. (1983), 16, 239–241.Google Scholar
2. Nakazawa, H. et. al. X-Ray Microscopy in Biology and Medicine, ed. by K, Shinohara et al., Japan Sci, Soc. Press, Tokyo/Verlin pp 81–86 (1990).Google Scholar
3. Nozaki, H. and Wakazawa, H., J. Appl. Cryst. (1986), 19, 453–455.10.1107/S0021889886088969Google Scholar
4. Sample supply: Prof, Kazuo Yamazaki and Prof, Izumi Hakai.Google Scholar
5. Rindby, A., “Application of Fiber Technique in the X-Ray Region,” Huclear Instruments arid Methods in Physics Research, A249 (1986) 536–540. (and many others from this group at Chalmers University, Sweden)Google Scholar
6. Carpenter, D. A. and Taylor, M, A., “Fast, High Resolution X-Ray Microfluorescence Imaging,” Adv. X-Ray Anal, 34 (1991), 217–221.Google Scholar