Field, micromorphological, pollen, whole soil (XRF), and stable isotope geochemical methods were used to evaluate the latest Pleistocene to Holocene climate record from a floodplain–terrace system in southeastern West Virginia. A late Pleistocene (22,940 ± 150 14C yr B.P.) silt paleosol with low-chroma colors formed from fluviolacustrine sediment deposited during the last glacial maximum (Wisconsinan) and records a cooler full-glacial paleoclimate. Fluvial gravel deposited between the latest Pleistocene and earliest Holocene (prior to 6360 ± 40 14C yr B.P.) was weathered in the middle Holocene under warmer, drier climate conditions, possibly correlated with the Hypsithermal and Altithermal Events of the eastern and southwestern United States, respectively. The glacial to interglacial climate shift is recorded by: (1) changes from a poorly drained landscape with fine-textured soil, characterized by high organic C and redoximorphic features related to Fe removal and concentration, to a well-drained, coarse-textured setting without gley and with significant argillic (Bt) horizon development; (2) changes from a high Zr and Ti silt-dominated parent material to locally derived, coarse fluvial gravels lower in Zr and Ti; (3) a shift from dominantly conifer and sedge pollen in the paleosol to a modern oak/hickory hardwood assemblage; and (4) a shift in δ13C values of soil organic matter from −28‰ to −24‰ PDB, suggesting an ecosystem shift from cooler, C3-dominated flora to one that was mixed C3 and C4, but still predominantly composed of C3 plants. A root-restrictive placic horizon developed between the late Pleistocene silt paleosol and the overlying fluvial gravel because of the high permeability contrast between the two textures of soil materials. This layer formed a barrier that effectively isolated the Pleistocene paleosol from later Holocene pedogenic processes.

Floodplain soil–paleosol successions are valuable archives for reconstructing Pleistocene–Holocene climate changes but have been relatively unstudied in the southern Appalachian region. Two soil profiles on a small floodplain in southeastern Tennessee, USA were described and sampled in detail using both pedological and geological approaches, including stable carbon isotope analysis of soil organic matter (SOM). Correlation between the 2 profiles was constrained by uncalibrated AMS14C ages of bulk humates, and using SOM δ13C values, both mobile and immobile elements. Four distinct 2.5–4‰ shifts towards less negative δ13C values for SOM suggest ∼ 300-yr cyclicity and transient warmer and drier climate events, with either water-stressed C3vegetation or as much as 35% C4plants present during the mid-Holocene. These postulated multi-episodic drier climate conditions have never before been documented in the southern Appalachian region and are tentatively correlated with mid-Holocene warming and drying in the eastern US, the nearly time-equivalent mid-Holocene events documented in Texas, the US High Plains and in the Gulf of Mexico. High rates of floodplain sediment accumulation (0.5–3 mm/yr), high clay content and maintenance of poorly drained soil conditions favor preservation of high-resolution climate archives in floodplain deposits by inhibiting oxidation and translocation of organic C.