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X-ray powder diffraction data for N,N-dimethyl-1H-benzo[d]imidazol-2-amine, C9H11N3

Published online by Cambridge University Press:  22 April 2021

Xia Lin
Affiliation:
Guangxi Medical College, Nanning530023, China Medical College, Guangxi University, Nanning530004, China College of Chemistry and Chemical Engineering, Guangxi University, Nanning530004, China
Dan-dan Chen
Affiliation:
Guangxi Medical College, Nanning530023, China
Xiao-hui Lin
Affiliation:
Guangxi Medical College, Nanning530023, China
An-tao Liu
Affiliation:
Guangxi Medical College, Nanning530023, China
Bao Zong
Affiliation:
Guangxi Medical College, Nanning530023, China
Lian-jia Zou*
Affiliation:
Guangxi Medical College, Nanning530023, China
*
a)Author to whom correspondence should be addressed. Electronic mail: [email protected]

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for N,N-dimethyl-1H-benzo[d]imidazol-2-amine, C9H11N3, are reported [a = 11.379(3) Å, b = 10.227(5) Å, c = 7.151(1) Å, α = 90°, β = 90°, γ = 90°, unit-cell volume V = 832.318 Å3, Z = 4, ρcal = 1.286 g cm−3, and space group P21212]. All measured lines were indexed and were consistent with the P21212 space group. No detectable impurities were observed.

Type
Data Report
Copyright
Copyright © The Author(s), 2021. Published by Cambridge University Press on behalf of International Centre for Diffraction Data

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References

Boultif, A. and Louër, D. (1991). “Indexing of powder diffraction patterns for low-symmetry lattices by the successive dichotomy method,” J. Appl. Crystallogr. 24, 987993.CrossRefGoogle Scholar
de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder patternJ. Appl. Crystallogr. 1, 108113.CrossRefGoogle Scholar
Kang, H., Bang, T. S., Lee, J. W., Lew, J. H., Eom, S. H., Li, K., and Choi, H. Y. (2012). “Protective effect of the methanol extract from Cryptotaenia japonica Hassk. against lipopolysaccharide-induced inflammation in vitro and in vivo,” BMC Complement. Altern. Med. 12, 199205.CrossRefGoogle ScholarPubMed
Liu, A. T., Zhang, T., and Liang, X. M. (2018). “Chemical constituents of Cryptotaenia japonica and toxicity to Hep G2,” J. Guihaia 38, 469474.Google Scholar
Lu, J., Xu, Y. Z., Yang, M. X., Fu, X. J., Luo, F. J., and Li, Z. H. (2015). “Optimization of ultrasound-assisted extraction of flavonoids from Cryptotaenia japonica Hassk. and evaluation of antioxidant activity,” J. Agric. Sci. (Toronto) 7, 138146.Google Scholar
Pawley, G. S. (1981). “Unit-cell refinement from powder diffraction scans,” J. Appl. Crystallogr. 14(6), 357361.CrossRefGoogle Scholar
Seong, Z. K., Lee, S. Y., Poudel, A., Oh, S. R., and Lee, H. K. (2016). “Constituents of Cryptotaenia japonica inhibit melanogenesis via CREB- and MAPK-associated signaling pathways in murine B16 melanoma cells,” Molecule 21, 12951305.CrossRefGoogle ScholarPubMed
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 6065.CrossRefGoogle Scholar
Yang, W. P. and Xia, T. Y. (2010). Newly Compiled Chinese Herbal Medicine map and Commonly Used Formulas (Guizhou Science and Technology Press, Guiyang, Guizhou province, China).Google Scholar