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A Novel Technique for Mixed-mode Thin Film Adhesion Measurement

Published online by Cambridge University Press:  11 February 2011

Junlan Wang ,
Nancy R. Sottos  and
Richard L. Weaver
Junlan Wang
Affiliation:
Department of Theoretical and Applied Mechanics, University of Illinois at Urbana-Champaign, 216 Talbot, 104 S. Wright, Urbana, IL 61801, USA.
Nancy R. Sottos
Affiliation:
Department of Theoretical and Applied Mechanics, University of Illinois at Urbana-Champaign, 216 Talbot, 104 S. Wright, Urbana, IL 61801, USA.
Richard L. Weaver
Affiliation:
Department of Theoretical and Applied Mechanics, University of Illinois at Urbana-Champaign, 216 Talbot, 104 S. Wright, Urbana, IL 61801, USA.
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Abstract

Guided by recent parametric studies of laser-induced tensile spallation, we successfully developed a new test method for studying mixed-mode interfacial failure of thin films. By allowing an initial longitudinal wave to mode convert at an oblique surface, a high amplitude shear wave is generated in a fused silica substrate and propagated toward the thin film surface. A shear wave was generated with amplitude large enough to fail an Al film/fused silica interface and the corresponding shear stress was calculated from high-speed interferometric displacement measurements. Examination of the interfaces failed under mixed-mode conditions revealed significant wrinkling and tearing of the film, in great contrast to blister patterns observed in similar Al films failed under tensile loading. Slightly higher interfacial strength was measured for the same Al film/fused silica substrate under mixed-mode loading than under tensile loading. The mixed-mode loading experiment developed in the current work provides a new tool to explore a range of thin film interfacial failure modes as well as the role of extrinsic effects such as residual stress, surface roughness, and imperfections.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 750: Symposium Y – Surface Engineering 2002–Synthesis, Characterization and Applications , 2002 , Y3.5
Copyright
Copyright © Materials Research Society 2003

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References

REFERENCES

1. Evans, A. and Hutchinson, J.W., Acta Metall. Mater. 43, 2507–2530 (1995).Google Scholar
2. Mittal, K.L., J. Adhesion Sci. Tech. 1 (3), 247–259 (1987).Google Scholar
3. Hull, T.R., Colligon, J.S. and Hill, A.E., Vacuum, 37, 327–330 (1987).Google Scholar
4. Kriese, M.D., Gerberich, W.W. and Moody, N.R., J. Mater. Res., 14 (7), 3007–3018 (1999).Google Scholar
5. Kriese, M.D., Gerberich, W.W., and Moody, N.R., J. Mater. Res., 14 (7), 3019–3026 (1999).Google Scholar
6. Kim, K.S. and Kim, J., J. Eng. Materials & Technol.-Trans. ASME, 110 (3), 266–73(1988).Google Scholar
7. Thouless, M.D., IBM J. Res. Develop. 38, 367–377 (1994).Google Scholar
8. Vossen, J.L., in Adhesion Measurement of Thin Films, Thick Films and Bulk Coatings. ASTM STP640, 122–133 (1978).Google Scholar
9. Gupta, V., Argon, A.S., Cornie, J.A. and Parks, D.M., Mater. Sci. Engg., A126, 105–117 (1990).Google Scholar
10. Gupta, V., Argon, A.S., Parks, D.M. and Cornie, J.A., J. Mech. Phys. Solids, 40, 141–180 (1992)Google Scholar
11. Yuan, J. and Gupta, V., J. Appl. Phys., 74, 2388–2396 (1993).Google Scholar
12. Gupta, V. and Yuan, J., J. Appl. Phys., 74, 2397–2404 (1993).Google Scholar
13. Yuan, J., Gupta, V. and Pronin, A., J. Appl. Phys., 74, 2405–2410 (1993).Google Scholar
14. Gupta, V., Yuan, J. and Pronin, A., J. Adhesion Sci. Technol., 8, 713–747 (1994).Google Scholar
15. Wang, J., Weaver, R.L. and Sottos, N.R., Experimental Mechanics 42 (1), 74–83 (2002).Google Scholar
16. Graff, K., Wave Motion in Elastic Solids. Dover, 1991.Google Scholar
17. Wang, J., Sottos, N.R. and Weaver, R.L., to appear in Experimental Mechanics (2003)Google Scholar
18. Wang, J., PhD. Thesis, University of Illinois at Urbana-Champaign, 2002.Google Scholar
19. Hutchinson, J.W. and Suo, Z., Advances in Applied Mechanics, 29, 63–191 (1992)Google Scholar