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Microstructure Analysis of a Carbon–Carbon Composite Using Argon Ion Etching

Published online by Cambridge University Press:  28 January 2005

Andreas Pfrang ,
Boris Reznik ,
Thomas Schimmel  and
Dagmar Gerthsen
Andreas Pfrang
Affiliation:
Institut für Angewandte Physik, Universität Karlsruhe (TH), D-76128 Karlsruhe, Germany
Boris Reznik
Affiliation:
Laboratorium für Elektronenmikroskopie, Universität Karlsruhe (TH), D-76128 Karlsruhe, Germany
Thomas Schimmel
Affiliation:
Institut für Angewandte Physik, Universität Karlsruhe (TH), D-76128 Karlsruhe, Germany
Dagmar Gerthsen
Affiliation:
Laboratorium für Elektronenmikroskopie, Universität Karlsruhe (TH), D-76128 Karlsruhe, Germany
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Abstract

The microstructure of carbon–carbon composites obtained by chemical vapor infiltration of a carbon fiber felt was comparatively studied by reflection light microscopy, transmission electron microscopy (TEM), scanning electron microscopy (SEM), atomic force microscopy (AFM), and laser scanning confocal microscopy (LSCM). Ar+ ion etching was used to reveal and distinguish structural units of the pyrolytic carbon matrix. Mechanically polished samples, polished and subsequently ion etched samples, and fractured samples were compared. The values of surface roughness and surface height after polishing or after polishing and subsequent etching determined by AFM and LSCM correlate well with the degree of texture of the matrix layers obtained by polarized light microscopy and selected area electron diffraction. The carbon matrix is composed of structural units or “cells,” which contain a carbon fiber and a sequence of several differently textured layers around each fiber. Within high-textured layers columnar grains are well recognizable using polarized reflection light microscopy and confocal microscopy. The size of depressions within high-textured carbon layers found by AFM after ion etching correlates well with the size of differently tilted domains detected by both TEM and SEM.

Keywords

reflection light microscopyatomic force microscopylaser scanning confocal microscopytransmission electron microscopyscanning electron microscopyargon ion etchingcarbon–carbon compositepyrolytic carbon
Type
MATERIALS APPLICATIONS
Information
Microscopy and Microanalysis , Volume 11 , Issue 1 , February 2005 , pp. 46 - 55
Copyright
© 2005 Microscopy Society of America

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References

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