Hostname: page-component-586b7cd67f-2brh9 Total loading time: 0 Render date: 2024-12-01T02:10:53.575Z Has data issue: false hasContentIssue false

Extension of HRTEM Resolution: Solving Structures of Grain Boundary and Interface Using Gerchberg-Saxton Algorithm and Blind Deconvolution

Published online by Cambridge University Press:  02 July 2020

F.-R. Chen
Affiliation:
Dept. of Engineering and System Science, National Tsing Hua University, Taiwan
H. Ichinose
Affiliation:
Dept. of Materials Science and Engineering, Tokyo University, Japan
J. J. Kai
Affiliation:
Dept. of Engineering and System Science, National Tsing Hua University, Taiwan
L. Chang
Affiliation:
Dept. of Materials and Engineering, National Chiao-Tong University, Taiwan
Get access

Abstract

Oxides, nitrides, carbides and silicides contain more than one type of atoms that gives one extra degree of freedom in the grain boundary and interfacial structure. This degree of freedom is the choice of the boundary plane containing different type of atoms which results of several structural multiplicities in the boundary. Coexistence of the structural multiplicities (or boundary domains) in the interface and grain boundary were reported [1, 2]. The structural information in high frequency domain is usually blurred and lost in the lens system of a high resolution transmission electron microscopes (HRTEM) such that the HRTEM image may not truly represent the real structure. Conventionally, the structures of grain boundary and interface were solved using forward method. The forward method involves matching the simulated images from guessed possible models with the through focal series experimental images. Recently, rereconstruction methods such as focal variation holography [3, 4], tiltbeam holography [5] and Gerchberg-Saxton algorithm [6] provide a backward (direct) way to recover the structural information lost in a modern microscope.

Type
Quantitative Transmission Electron Microscopy of Interfaces (Organized by M. Rüehle, Y. Zhu and U. Dahmen)
Copyright
Copyright © Microscopy Society of America 2001

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

[1]Chen, W J and Chen, F-R, Philos. Mag. 68A: (1993) 605630CrossRefGoogle Scholar
[2]Chen, F. R., Chu, C. C., Wang, J. Y. and Chang, L., Phil. Mag. 72, (1995) 529544CrossRefGoogle Scholar
[3]Coene, W., Janssen, A. J. E. M, Op de Beeck, M. and Van Dyck, D., Philips Electron Optics Bulletin 132(1995) 1528Google Scholar
[4]Thust, A., Coene, W.,Op de Beeck, M. and Van Dyck, D., Ultramicroscopy, 64 (1994) 211230CrossRefGoogle Scholar
[5]Kirkland, A. I., W. O.|Saxton, Chau, K.-L., Tsuno, K. and Kawasaki, M., Ultramicroscopy, 57 (1995) 355374CrossRefGoogle Scholar
[6]Chen, F.-R., J J, Kai, L, Chang, Wang, J Y and Chen, W J, J. of Electron Microscopy 48: (1999) 827836CrossRefGoogle Scholar
[7]Gerchberg, R. W. and Saxton, W. O., Optik, 35 (1972) 237246Google Scholar