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Electron Backscatter Diffraction and Transmission Kikuchi Diffraction Analysis of an Austenitic Stainless Steel Subjected to Surface Mechanical Attrition Treatment and Plasma Nitriding

Published online by Cambridge University Press:  03 July 2015

Gwénaëlle Proust ,
Delphine Retraint ,
Mahdi Chemkhi ,
Arjen Roos  and
Clemence Demangel
Gwénaëlle Proust*
Affiliation:
School of Civil Engineering, The University of Sydney, NSW 2006, Australia
Delphine Retraint
Affiliation:
Charles Delaunay Institute, University of Technology of Troyes (UTT), LASMIS, UMR STMR CNRS 6279, 12 rue Marie Curie, CS 42060, 10004 Troyes Cedex, France
Mahdi Chemkhi
Affiliation:
Charles Delaunay Institute, University of Technology of Troyes (UTT), LASMIS, UMR STMR CNRS 6279, 12 rue Marie Curie, CS 42060, 10004 Troyes Cedex, France
Arjen Roos
Affiliation:
Charles Delaunay Institute, University of Technology of Troyes (UTT), LASMIS, UMR STMR CNRS 6279, 12 rue Marie Curie, CS 42060, 10004 Troyes Cedex, France
Clemence Demangel
Affiliation:
CRITT-MDTS, 3 bd J. Delautre, 08000 Charleville-Mézières, France
*
*Corresponding author. [email protected]
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Abstract

Austenitic 316L stainless steel can be used for orthopedic implants due to its biocompatibility and high corrosion resistance. Its range of applications in this field could be broadened by improving its wear and friction properties. Surface properties can be modified through surface hardening treatments. The effects of such treatments on the microstructure of the alloy were investigated here. Surface Mechanical Attrition Treatment (SMAT) is a surface treatment that enhances mechanical properties of the material surface by creating a thin nanocrystalline layer. After SMAT, some specimens underwent a plasma nitriding process to further enhance their surface properties. Using electron backscatter diffraction, transmission Kikuchi diffraction, energy dispersive spectroscopy, and transmission electron microscopy, the microstructural evolution of the stainless steel after these different surface treatments was characterized. Microstructural features investigated include thickness of the nanocrystalline layer, size of the grains within the nanocrystalline layer, and depth of diffusion of nitrogen atoms within the material.

Keywords

stainless steelsurface mechanical attrition treatment (SMAT)plasma nitridingelectron backscatter diffraction (EBSD)transmission Kikuchi diffraction (TKD)severe plastic deformation
Type
Materials Applications and Techniques
Information
Microscopy and Microanalysis , Volume 21 , Issue 4 , August 2015 , pp. 919 - 926
Copyright
© Microscopy Society of America 2015 

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References

Basa, A., Thaulow, C. & Barnoush, A. (2014). Chemically induced phase transformation in austenite by focused ion beam. Metall Mater Trans A 45, 1189–1198.CrossRefGoogle Scholar
Bell, T. (2002). Surface modifications of austenitic stainless steels. Surf Eng 18(6), 415–422.CrossRefGoogle Scholar
Buhagiar, J., Dong, H. & Bell, T. (2007). Low temperature plasma surface alloying of medical grade austenitic stainless steel with carbon and nitrogen. Surf Eng 23(4), 313–317.CrossRefGoogle Scholar
Chemkhi, M., Retraint, D., Montay, G., Garnier, C. & Belahcene, F. (2011). Effect of SMAT Parameters on Microstructural Features using DOE Technique. International Conference on Shot Peening-11. South Bend, Indiana, USA.Google Scholar
Chemkhi, M., Retraint, D., Roos, A., Demangel, C., Proust, G. & Waltz, L. (2012). Microstructural evolution of a 316L alloy subjected to surface nanocrystallisation and low-temperature plasma nitriding. 15th International Conference on Advances in Materials and Processing Technologies, Wollongong, NSW, Australia.Google Scholar
Chemkhi, M., Retraint, D., Roos, A., Garnier, C., Waltz, L., Demangel, C. & Proust, G. (2013). The effect of surface mechanical attrition treatment on low temperature plasma nitriding of an austenitic stainless steel. Surf Coat Tech 221, 191–195.Google Scholar
Dong, H. (2010). S-phase surface engineering of Fe-Cr, Co-Cr and Ni-Cr alloys. Inter Mater Rev 55(2), 65–98.Google Scholar
Egawa, M., Ueda, N., Nakata, K., Tsujikawa, M. & Tanaka, M. (2010). Effect of additive alloying element on plasma nitriding and carburizing behavior for austenitic stainless steels. Surf Coat Tech 205(Suppl 1(0)), S246–S251.Google Scholar
Li, C.X. & Bell, T. (2004). Sliding wear properties of active screen plasma nitrided 316 austenitic stainless steel. Wear 256(11–12), 1144–1152.CrossRefGoogle Scholar
Lin, Y., Lu, J., Wang, L., Xu, T. & Xue, Q. (2006). Surface nanocrystallization by surface mechanical attrition treatment and its effect on structure and properties of plasma nitrided AISI 321 stainless steel. Acta Mater 54(20), 5599–5605.CrossRefGoogle Scholar
Liu, S., Gao, S.Y., Zhou, Y.F., Xing, X.L., Hou, X.R., Yang, Y.L. & Yang, Q.X. (2014). A research on the microstructure evolution of austenite stainless steel by surface mechanical attrition treatment. Mater Sci Eng A-Struct 617(0), 127–138.CrossRefGoogle Scholar
Lu, K. & Lu, J. (2004). Nanostructured surface layer on metallic materials induced by surface mechanical attrition treatment. Mater Sci Eng A-Struct 375–377, 38–45.CrossRefGoogle Scholar
Ratner, B.D., Hoffman, A.S., Schoen, F.J. & Lemons, J.E. Eds (2013). Biomaterials Science : An Introduction to Materials in Medicine . San Diego, CA, USA: Elsevier Science.Google Scholar
Samih, Y., Beausir, B., Bolle, B. & Grosdidier, T. (2013). In-depth quantitative analysis of the microstructures produced by Surface Mechanical Attrition Treatment (SMAT). Mater Charact 83, 129–138.CrossRefGoogle Scholar
Thaiwatthana, S., Li, X.Y., Dong, H. & Bell, T. (2002). Comparison studies on properties of nitrogen and carbon S phase on low temperature plasma alloyed AISI 316 stainless steel. Surf Eng 18(6), 433–437.Google Scholar
Tong, W.P., Liu, C.Z., Wang, W., Tao, N.R., Wang, Z.B., Zuo, L. & He, J.C. (2007). Gaseous nitriding of iron with a nanostructured surface layer. Scripta Mater 57(6), 533–536.CrossRefGoogle Scholar
Trimby, P.W. (2012). Orientation mapping of nanostructured materials using transmission Kikuchi diffraction in the scanning electron microscope. Ultramicroscopy 120, 16–24.Google Scholar
Trindade, V.B., Krupp, U., Hanjari, B.Z., Yang, S. & Christ, H.J. (2005). Effect of alloy grain size on the high-temperature oxidation behavior of the austenitic steel TP 347. Mater Res 8, 371–375.Google Scholar
Waltz, L., Retraint, D., Roos, A., Garnier, C. & Olier, P. (2011). Effect of interfacial oxidation occurring during the duplex process combining surface nanocrystallisation and co-rolling. Surf Coat Tech 205, 4608–4613.Google Scholar
Xu, X.L., Wang, L., Yu, Z.W. & Hei, Z.K. (2000). Microstructural characterization of plasma nitrided austenitic stainless steel. Surf Coat Tech 132(2–3), 270–274.CrossRefGoogle Scholar